Technology Process of 2-(2-methoxynaphthalen-1-yl)cyclohexanone
There total 4 articles about 2-(2-methoxynaphthalen-1-yl)cyclohexanone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
formic acid; palladium diacetate; 1,2-bis-(diphenylphosphino)ethane;
In
1,4-dioxane;
at 40 ℃;
for 10h;
Inert atmosphere;
Schlenk technique;
DOI:10.1021/jo5014806
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydride / tetrahydrofuran; mineral oil / 16 h / 40 °C / Inert atmosphere; Schlenk technique
2: pyridine / chloroform / 18 h / 40 °C / Inert atmosphere; Schlenk technique
3: palladium diacetate; formic acid; 1,2-bis-(diphenylphosphino)ethane / 1,4-dioxane / 10 h / 40 °C / Inert atmosphere; Schlenk technique
With
pyridine; formic acid; palladium diacetate; sodium hydride; 1,2-bis-(diphenylphosphino)ethane;
In
tetrahydrofuran; 1,4-dioxane; chloroform; mineral oil;
1: |Dieckmann Condensation;
DOI:10.1021/jo5014806
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine / chloroform / 18 h / 40 °C / Inert atmosphere; Schlenk technique
2: palladium diacetate; formic acid; 1,2-bis-(diphenylphosphino)ethane / 1,4-dioxane / 10 h / 40 °C / Inert atmosphere; Schlenk technique
With
pyridine; formic acid; palladium diacetate; 1,2-bis-(diphenylphosphino)ethane;
In
1,4-dioxane; chloroform;
DOI:10.1021/jo5014806
