1-(Benzyloxycarbonylamino)-1-deoxy-2,3-O-isopropylidene-1-(2-thiazolyl)-D-threo-triitol

Base Information

Chemical Name:1-(Benzyloxycarbonylamino)-1-deoxy-2,3-O-isopropylidene-1-(2-thiazolyl)-D-threo-triitol
CAS No.:172944-99-9
Molecular Formula:C₁₇H₂₀N₂O₄S
Molecular Weight:348.423
Hs Code.:

Synonyms:1-(Benzyloxycarbonylamino)-1-deoxy-2,3-O-isopropylidene-1-(2-thiazolyl)-D-threo-triitol

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Chemical Property of 1-(Benzyloxycarbonylamino)-1-deoxy-2,3-O-isopropylidene-1-(2-thiazolyl)-D-threo-triitol

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Technology Process of 1-(Benzyloxycarbonylamino)-1-deoxy-2,3-O-isopropylidene-1-(2-thiazolyl)-D-threo-triitol

There total 4 articles about 1-(Benzyloxycarbonylamino)-1-deoxy-2,3-O-isopropylidene-1-(2-thiazolyl)-D-threo-triitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 143539-88-2
C-[(S)-C-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-C-thiazol-2-yl]-methylamine

: 172944-99-9
1-(Benzyloxycarbonylamino)-1-deoxy-2,3-O-isopropylidene-1-(2-thiazolyl)-D-threo-triitol

Guidance literature:: With sodium hydrogencarbonate; In 1,4-dioxane; at 0 ℃; for 0.333333h; Yield given;

Reference yield:

: 91190-38-4,111058-38-9,1165677-00-8
N-benzyl-2,3-O-isopropylidene-D-glyceraldehyde nitrone

: 172944-99-9
1-(Benzyloxycarbonylamino)-1-deoxy-2,3-O-isopropylidene-1-(2-thiazolyl)-D-threo-triitol

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / diethyl ether; tetrahydrofuran; hexane / 1.) -78 deg C, 15 min, 2.) -80 deg C, 15 min

2: 20percent aq. TiCl₃ / methanol / 0.25 h / Ambient temperature

3: 7percent aq. NaHCO₃ / dioxane / 0.33 h / 0 °C

With titanium(III) chloride; sodium hydrogencarbonate; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; hexane;

Reference yield:

: 143539-87-1
N-Benzyl-1-deoxy-1-(hydroxyamino)-2,3-O-isopropylidene-1-(2-thiazolyl)-D-threo-triitol

: 172944-99-9
1-(Benzyloxycarbonylamino)-1-deoxy-2,3-O-isopropylidene-1-(2-thiazolyl)-D-threo-triitol

Guidance literature:: Multi-step reaction with 2 steps

1: 20percent aq. TiCl₃ / methanol / 0.25 h / Ambient temperature

2: 7percent aq. NaHCO₃ / dioxane / 0.33 h / 0 °C

With titanium(III) chloride; sodium hydrogencarbonate; In 1,4-dioxane; methanol;