2-[4-N-(o-methoxyphenyl)-N-methylaminopiperidinyl]-N-pyridin-2-ylacetamide

Base Information

Chemical Name:2-[4-N-(o-methoxyphenyl)-N-methylaminopiperidinyl]-N-pyridin-2-ylacetamide
CAS No.:260360-18-7
Molecular Formula:C₂₀H₂₆N₄O₂
Molecular Weight:354.452
Hs Code.:

Synonyms:2-[4-N-(o-methoxyphenyl)-N-methylaminopiperidinyl]-N-pyridin-2-ylacetamide

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Chemical Property of 2-[4-N-(o-methoxyphenyl)-N-methylaminopiperidinyl]-N-pyridin-2-ylacetamide

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Technology Process of 2-[4-N-(o-methoxyphenyl)-N-methylaminopiperidinyl]-N-pyridin-2-ylacetamide

There total 1 articles about 2-[4-N-(o-methoxyphenyl)-N-methylaminopiperidinyl]-N-pyridin-2-ylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 2-[4-N-(o-methoxyphenyl)aminopiperidinyl]-N-pyridin-2-ylacetamide hydrochloride

: 260360-18-7
2-[4-N-(o-methoxyphenyl)-N-methylaminopiperidinyl]-N-pyridin-2-ylacetamide

Guidance literature:: With hydrogen; 20percent Pd(OH)2/C; In ethanol; at 60 ℃; for 18h; under 3102.97 Torr;
DOI:10.1021/jm991088y

Reference yield: 90.0%

: 260360-18-7
2-[4-N-(o-methoxyphenyl)-N-methylaminopiperidinyl]-N-pyridin-2-ylacetamide

: 260360-19-8
2-[4-N-(o-methoxyphenyl)-N-methylaminopiperidinyl]-N-pyridin-2-ylamine

Guidance literature:: With diisobutylaluminium hydride; In diethyl ether; toluene; at 20 ℃; for 18h;
DOI:10.1021/jm991088y

Reference yield:

: 260360-18-7
2-[4-N-(o-methoxyphenyl)-N-methylaminopiperidinyl]-N-pyridin-2-ylacetamide

: cyclohexanecarboxylic acid (2-{4-[(2-methoxy-phenyl)-methyl-amino]-piperidin-1-yl}-ethyl)-pyridin-2-yl-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / DIBAL-H / diethyl ether; toluene / 18 h / 20 °C

2: 62 percent / Et₃N / CH₂Cl₂ / 2 h / 20 °C

With diisobutylaluminium hydride; triethylamine; In diethyl ether; dichloromethane; toluene; 1: Reduction / 2: Acylation;
DOI:10.1021/jm991088y