1-(3-bromopropyl)-2-methoxycyclohexa-2,5-dienecarboxylic acid tert-butyl ester

Base Information

• Chemical Name: 1-(3-bromopropyl)-2-methoxycyclohexa-2,5-dienecarboxylic acid tert-butyl ester
• CAS No.: 1045729-62-1
• Molecular Formula: C₁₅H₂₃BrO₃
• Molecular Weight: 331.25

Synonyms:1-(3-bromopropyl)-2-methoxycyclohexa-2,5-dienecarboxylic acid tert-butyl ester

Chemical Property of 1-(3-bromopropyl)-2-methoxycyclohexa-2,5-dienecarboxylic acid tert-butyl ester

Chemical Property:

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Technology Process of 1-(3-bromopropyl)-2-methoxycyclohexa-2,5-dienecarboxylic acid tert-butyl ester

There total 1 articles about 1-(3-bromopropyl)-2-methoxycyclohexa-2,5-dienecarboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

tert-butyl 2-methoxybenzoate (16537-20-5) + 1,3-dibromo-propane (109-64-8) → 1-(3-bromopropyl)-2-methoxycyclohexa-2,5-dienecarboxylic acid tert-butyl ester (1045729-62-1)

Guidance literature:

tert-butyl 2-methoxybenzoate; With ammonia; sodium; lithium; In tetrahydrofuran; water; tert-butyl alcohol; at -78 ℃; Inert atmosphere;

1,3-dibromo-propane; In tetrahydrofuran; water; tert-butyl alcohol; at -78 ℃; Inert atmosphere;

DOI:10.1039/b803308k

Reference yield: 74.0%

1-(3-bromopropyl)-2-methoxycyclohexa-2,5-dienecarboxylic acid tert-butyl ester (1045729-62-1) → 1-(3-bromopropyl)-2-methoxy-4-oxocyclohexa-2,5-diene-carboxylic acid tert-butyl ester (1045729-64-3)

Guidance literature:

With tert.-butylhydroperoxide; pyridinium dichromate; Celite; In benzene;

DOI:10.1039/b803308k

upstream raw materials:

tert-butyl 2-methoxybenzoate

1,3-dibromo-propane

Downstream raw materials:

1-(3-bromopropyl)-2-methoxy-4-oxocyclohexa-2,5-diene-carboxylic acid tert-butyl ester

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