C₅H₅FeC₆(CH₃)5NHCOC₆H₅⁽¹⁺⁾*PF₆^(1-)=C₅H₅FeC₆(CH₃)5NHCOC₆H₅PF₆

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Chemical Name:C₅H₅FeC₆(CH₃)5NHCOC₆H₅⁽¹⁺⁾*PF₆^(1-)=C₅H₅FeC₆(CH₃)5NHCOC₆H₅PF₆
CAS No.:83292-60-8
Molecular Formula:C₂₃H₂₆FeNO*F₆P
Molecular Weight:533.277
Hs Code.:

C<sub>5</sub>H<sub>5</sub>FeC<sub>6</sub>(CH<sub>3</sub>)5NHCOC<sub>6</sub>H<sub>5</sub><sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=C<sub>5</sub>H<sub>5</sub>FeC<sub>6</sub>(CH<sub>3</sub>)5NHCOC<sub>6</sub>H<sub>5</sub>PF<sub>6</sub>

Synonyms:C₅H₅FeC₆(CH₃)5NHCOC₆H₅⁽¹⁺⁾*PF₆^(1-)=C₅H₅FeC₆(CH₃)5NHCOC₆H₅PF₆

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Chemical Property of C₅H₅FeC₆(CH₃)5NHCOC₆H₅⁽¹⁺⁾*PF₆^(1-)=C₅H₅FeC₆(CH₃)5NHCOC₆H₅PF₆

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Technology Process of C₅H₅FeC₆(CH₃)5NHCOC₆H₅⁽¹⁺⁾*PF₆^(1-)=C₅H₅FeC₆(CH₃)5NHCOC₆H₅PF₆

There total 1 articles about C₅H₅FeC₆(CH₃)5NHCOC₆H₅⁽¹⁺⁾*PF₆^(1-)=C₅H₅FeC₆(CH₃)5NHCOC₆H₅PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 82879-24-1
[η5-C5H5Fe-η5-C6(CH3)5NH2]+PF6-

: 98-88-4
benzoyl chloride

: 83292-60-8
C₅H₅FeC₆(CH₃)5NHCOC₆H₅⁽¹⁺⁾*PF₆^(1-)=C₅H₅FeC₆(CH₃)5NHCOC₆H₅PF₆

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; t-BuOK added to a suspn. of complex in two portions, stirred for 5 min,room temperature, addition of obtained soln. to chloranhydride at 5°C, stirred for 1 h, molar ratio of t-BuOk/anhydride/complex 2/1/1, addition of dilute HPF6, N2 atm.; evapn. in vac., treatment with aq. Na2CO3, filtration, addition of 60% HPF6 to filtrate, filtration, drying on filtre, dissolving in a minimum of acetone, filtration, pptn. with ether; elem. anal.;
DOI:10.1016/S0022-328X(00)92892-4