C₂₄H₃₇NO₃SSi

Base Information

Chemical Name:C₂₄H₃₇NO₃SSi
CAS No.:1436715-89-7
Molecular Formula:C₂₄H₃₇NO₃SSi
Molecular Weight:447.714
Hs Code.:

C<sub>24</sub>H<sub>37</sub>NO<sub>3</sub>SSi

Synonyms:C₂₄H₃₇NO₃SSi

Suppliers and Price of C₂₄H₃₇NO₃SSi

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₄H₃₇NO₃SSi

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₄H₃₇NO₃SSi

There total 7 articles about C₂₄H₃₇NO₃SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 930-68-7
cyclohexenone

: 1436715-89-7
C₂₄H₃₇NO₃SSi

Guidance literature:: Multi-step reaction with 7 steps

1: barium(II) hydroxide / methanol; water; 1-methyl-pyrrolidin-2-one / 4 h / 29 °C / Inert atmosphere

2: triethylamine / dichloromethane / 6 h / 30 °C / Inert atmosphere

3: cerium(III) chloride heptahydrate; sodium tetrahydroborate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

4: triethylamine; dmap / dichloromethane / 12 h / Inert atmosphere; Reflux

5: potassium carbonate / methanol / 1 h / 30 °C / Inert atmosphere

6: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 °C / Inert atmosphere

7: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / 12 h / 40 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; cerium(III) chloride heptahydrate; di-isopropyl azodicarboxylate; potassium carbonate; triethylamine; triphenylphosphine; barium(II) hydroxide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane; water; 1: |Baylis-Hillman Reaction;
DOI:10.1021/jo400634c

Reference yield:

: 105956-40-9
2-(hydroxymethyl)cyclohex-2-en-1-one

: 1436715-89-7
C₂₄H₃₇NO₃SSi

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / dichloromethane / 6 h / 30 °C / Inert atmosphere

2: cerium(III) chloride heptahydrate; sodium tetrahydroborate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3: triethylamine; dmap / dichloromethane / 12 h / Inert atmosphere; Reflux

4: potassium carbonate / methanol / 1 h / 30 °C / Inert atmosphere

5: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 °C / Inert atmosphere

6: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / 12 h / 40 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; cerium(III) chloride heptahydrate; di-isopropyl azodicarboxylate; potassium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo400634c

Reference yield:

: 106281-44-1
(6-oxocyclohex-1-en-1-yl)methyl acetate

: 1436715-89-7
C₂₄H₃₇NO₃SSi

Guidance literature:: Multi-step reaction with 5 steps

1: cerium(III) chloride heptahydrate; sodium tetrahydroborate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2: triethylamine; dmap / dichloromethane / 12 h / Inert atmosphere; Reflux

3: potassium carbonate / methanol / 1 h / 30 °C / Inert atmosphere

4: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 °C / Inert atmosphere

5: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / 12 h / 40 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; cerium(III) chloride heptahydrate; di-isopropyl azodicarboxylate; potassium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo400634c