Technology Process of C34H42O5S2
There total 4 articles about C34H42O5S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C27H36O5S2;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
for 0.666667h;
Cooling with ice;
benzyl bromide;
In
N,N-dimethyl-formamide; mineral oil;
Cooling with ice;
DOI:10.1002/ejoc.201201184
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium; triphenylmethane / hexane; tetrahydrofuran / 2 h / -78 - -20 °C / Inert atmosphere
1.2: -78 - -20 °C
2.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.67 h / Cooling with ice
2.2: Cooling with ice
With
n-butyllithium; triphenylmethane; sodium hydride;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/ejoc.201201184
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.67 h / Cooling with ice
1.2: Cooling with ice
2.1: n-butyllithium; triphenylmethane / hexane; tetrahydrofuran / 2 h / -78 - -20 °C / Inert atmosphere
2.2: -78 - -20 °C
3.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.67 h / Cooling with ice
3.2: Cooling with ice
With
n-butyllithium; triphenylmethane; sodium hydride;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/ejoc.201201184