N-(2-Chlorobenzylidene)-4-methoxyaniline

Base Information

Chemical Name:N-(2-Chlorobenzylidene)-4-methoxyaniline
CAS No.:17099-11-5
Molecular Formula:C₁₄H₁₂ClNO
Molecular Weight:245.708
Hs Code.:
European Community (EC) Number:621-400-7
DSSTox Substance ID:DTXSID20361645
Nikkaji Number:J1.196.489C
Mol file:17099-11-5.mol

Synonyms:N-(2-Chlorobenzylidene)-4-methoxyaniline;17099-11-5;1-(2-chlorophenyl)-N-(4-methoxyphenyl)methanimine;N-(2-CHLOROBENZYLIDENE)-4-ANISIDINE;N-(2-CHLOROBENZYLIDENE)-4-METHOXYANILIN;SCHEMBL12416597;DTXSID20361645;N-p-Anisyl-2-chlorobenzenemethanimine;AKOS004909618;N-(2-Chlorobenzylidene)-4-methoxyaniline, 97%;J-010679;N-[(E)-(2-chlorophenyl)methylidene]-4-methoxyaniline;(E)-1-(2-Chlorophenyl)-N-(4-methoxyphenyl)methanimine

Suppliers and Price of N-(2-Chlorobenzylidene)-4-methoxyaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
N-(2-CHLOROBENZYLIDENE)-P-ANISIDINE AldrichCPR
250mg
$ 144.00

Sigma-Aldrich
N-(2-Chlorobenzylidene)-4-methoxyaniline 97%
5g
$ 96.40

American Custom Chemicals Corporation
N-(2-CHLOROBENZYLIDENE)-4-METHOXYANILINE 95.00%
5G
$ 891.01

American Custom Chemicals Corporation
N-(2-CHLOROBENZYLIDENE)-4-METHOXYANILINE 95.00%
1G
$ 634.15

Total 6 raw suppliers

Chemical Property of N-(2-Chlorobenzylidene)-4-methoxyaniline

Chemical Property:

Vapor Pressure:8.26E-06mmHg at 25°C
Melting Point:61-65 °C(lit.)
Refractive Index:1.555
Boiling Point:385.8°C at 760 mmHg
Flash Point:187.1°C
PSA：21.59000
Density:1.11g/cm³
LogP:4.09920
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:245.0607417
Heavy Atom Count:17
Complexity:249

Purity/Quality:

98%,99%, ^*data from raw suppliers

N-(2-CHLOROBENZYLIDENE)-P-ANISIDINE AldrichCPR ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi
Statements: 37/38-41
Safety Statements: 26-36/37/39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)N=CC2=CC=CC=C2Cl

Technology Process of N-(2-Chlorobenzylidene)-4-methoxyaniline

There total 9 articles about N-(2-Chlorobenzylidene)-4-methoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 100-17-4
para-methoxynitrobenzene

: 17849-38-6
2-Chlorobenzyl alcohol

: 17099-11-5,83306-64-3,83306-69-8
N-(4-methoxyphenyl)-2-chlorobenzylidenimine

Guidance literature:: With potassium phosphate monohydrate; trimethylamine-N-oxide; C₁₈H₂₇FeO₄Si₂; In toluene; at 140 ℃; for 20h; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1021/acs.joc.0c02505

Reference yield: 86.0%

: 17099-11-5,83306-64-3,83306-69-8
N-(4-methoxyphenyl)-2-chlorobenzylidenimine

Guidance literature:

Reference yield: 85.0%

: 89-98-5
2-chloro-benzaldehyde

: 104-94-9
4-methoxy-aniline

: 17099-11-5,83306-64-3,83306-69-8
N-(4-methoxyphenyl)-2-chlorobenzylidenimine

Guidance literature:: With sulfuric acid; In neat (no solvent); Microwave irradiation; Sealed tube; Green chemistry;
DOI:10.1016/j.saa.2012.09.039