2-(allyloxy)phenyl phenyl sulfide

Base Information

• Chemical Name: 2-(allyloxy)phenyl phenyl sulfide
• CAS No.: 1443143-42-7
• Molecular Formula: C₁₅H₁₄OS
• Molecular Weight: 242.342
• Mol file: 1443143-42-7.mol

Synonyms:2-(allyloxy)phenyl phenyl sulfide

Chemical Property of 2-(allyloxy)phenyl phenyl sulfide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 2-(allyloxy)phenyl phenyl sulfide

There total 4 articles about 2-(allyloxy)phenyl phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

1-allyloxy-2-iodobenzene (24892-63-5) + C108H125CuN2O8S → 2-(allyloxy)phenyl phenyl sulfide (1443143-42-7)

Guidance literature:

In toluene; at 110 ℃; for 4h; Inert atmosphere;

DOI:10.1039/c5cc09232a

Reference yield: 80.0%

1-allyloxy-2-iodobenzene (24892-63-5) + sodium thiophenolate (930-69-8) → 2-(allyloxy)phenyl phenyl sulfide (1443143-42-7)

Guidance literature:

With 1,5-(2,9-dimethyl-1,10-phenanthroyl)-p-tert-butylcalix[8]arene; copper(l) chloride; In toluene; at 110 ℃; for 15h; Schlenk technique; Glovebox; Inert atmosphere;

DOI:10.1039/c5cc09232a

Reference yield: 16.0%

1-allyloxy-2-iodobenzene (24892-63-5) + thiophenol (108-98-5) → 2-(allyloxy)phenyl phenyl sulfide (1443143-42-7)

Guidance literature:

With copper(l) iodide; sodium t-butanolate; In acetonitrile; at 60 ℃; for 72h; Inert atmosphere; Sealed tube; Darkness;

DOI:10.1021/ja404050f

upstream raw materials:

1-allyloxy-2-iodobenzene

thiophenol

sodium thiophenolate