N⁽¹⁾-benzenesulfonyl-N⁽⁴⁾-(2-fluoro-1-iminoethyl)-1,4-diaminobutane*TFA

Base Information

Chemical Name:N⁽¹⁾-benzenesulfonyl-N⁽⁴⁾-(2-fluoro-1-iminoethyl)-1,4-diaminobutane*TFA
CAS No.:1335096-44-0
Molecular Formula:C₂HF₃O₂*C₁₂H₁₈FN₃O₂S
Molecular Weight:401.382
Hs Code.:

N<sup>(1)</sup>-benzenesulfonyl-N<sup>(4)</sup>-(2-fluoro-1-iminoethyl)-1,4-diaminobutane*TFA

Synonyms:N⁽¹⁾-benzenesulfonyl-N⁽⁴⁾-(2-fluoro-1-iminoethyl)-1,4-diaminobutane*TFA

Suppliers and Price of N⁽¹⁾-benzenesulfonyl-N⁽⁴⁾-(2-fluoro-1-iminoethyl)-1,4-diaminobutane*TFA

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N⁽¹⁾-benzenesulfonyl-N⁽⁴⁾-(2-fluoro-1-iminoethyl)-1,4-diaminobutane*TFA

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Technology Process of N⁽¹⁾-benzenesulfonyl-N⁽⁴⁾-(2-fluoro-1-iminoethyl)-1,4-diaminobutane*TFA

There total 2 articles about N⁽¹⁾-benzenesulfonyl-N⁽⁴⁾-(2-fluoro-1-iminoethyl)-1,4-diaminobutane*TFA which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: ethyl 2-fluorothioacetimidate

: 1335096-56-4
N⁽¹⁾-benzenesulfonyl-1,4-diaminobutane*TFA

: 1335096-44-0
N⁽¹⁾-benzenesulfonyl-N⁽⁴⁾-(2-fluoro-1-iminoethyl)-1,4-diaminobutane*TFA

Guidance literature:: With caesium carbonate; In methanol; at 20 ℃;
DOI:10.1021/jm2008985

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 1335096-44-0
N⁽¹⁾-benzenesulfonyl-N⁽⁴⁾-(2-fluoro-1-iminoethyl)-1,4-diaminobutane*TFA

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / 1,4-dioxane; water / 20 °C

2: 0.5 h / 0 °C

3: caesium carbonate / methanol / 20 °C

With sodium carbonate; caesium carbonate; In 1,4-dioxane; methanol; water;
DOI:10.1021/jm2008985