methyl 2-acetamido-4,6-O-benzylidene-3-O-(tert-butyldimethylsilyl)-2-deoxy-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2-acetamido-4,6-O-benzylidene-3-O-(tert-butyldimethylsilyl)-2-deoxy-α-D-glucopyranoside
CAS No.:1214746-57-2
Molecular Formula:C₂₂H₃₅NO₆Si
Molecular Weight:437.608
Hs Code.:

Synonyms:methyl 2-acetamido-4,6-O-benzylidene-3-O-(tert-butyldimethylsilyl)-2-deoxy-α-D-glucopyranoside

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Chemical Property of methyl 2-acetamido-4,6-O-benzylidene-3-O-(tert-butyldimethylsilyl)-2-deoxy-α-D-glucopyranoside

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Technology Process of methyl 2-acetamido-4,6-O-benzylidene-3-O-(tert-butyldimethylsilyl)-2-deoxy-α-D-glucopyranoside

There total 1 articles about methyl 2-acetamido-4,6-O-benzylidene-3-O-(tert-butyldimethylsilyl)-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 6619-02-9,6619-04-1,10300-76-2,16727-56-3,17327-07-0,28978-56-5,52885-36-6,52885-45-7,78216-83-8,78513-50-5,87038-18-4,88295-36-7,110508-78-6,113159-04-9,117064-54-7,128657-61-4,129784-17-4,137330-28-0,78216-82-7
methyl N-acetyl-2-amino-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

: 1214746-57-2
methyl 2-acetamido-4,6-O-benzylidene-3-O-(tert-butyldimethylsilyl)-2-deoxy-α-D-glucopyranoside

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 36h; Inert atmosphere;
DOI:10.1021/jo9026098

Reference yield: 87.0%

: 1214746-57-2
methyl 2-acetamido-4,6-O-benzylidene-3-O-(tert-butyldimethylsilyl)-2-deoxy-α-D-glucopyranoside

: 1214746-59-4
methyl 2-acetamido-4-O-benzoyl-3-O-(tert-butyldimethylsilyl)-2-deoxy-α-D-glucopyranoside

: C₂₂H₃₅NO₇Si

Guidance literature:: With 3,3-dimethyldioxirane; In acetone; at 5 ℃; for 96h; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo9026098

Reference yield:

: 1214746-57-2
methyl 2-acetamido-4,6-O-benzylidene-3-O-(tert-butyldimethylsilyl)-2-deoxy-α-D-glucopyranoside

: C₂₂H₃₃NO₈Si

Guidance literature:: With sodium periodate; ruthenium(III) chloride trihydrate; In tetrachloromethane; water; acetonitrile; at 20 ℃; for 4h; regioselective reaction;
DOI:10.1002/chem.201503998