(1'R,2'R,3'S)-2-<2'-(2''-nitrophenylselanylmethyl)-3'-methylcyclopentyl>propan-2-ol

Base Information

Chemical Name:(1'R,2'R,3'S)-2-<2'-(2''-nitrophenylselanylmethyl)-3'-methylcyclopentyl>propan-2-ol
CAS No.:162460-45-9
Molecular Formula:C₁₆H₂₃NO₃Se
Molecular Weight:356.324
Hs Code.:

Synonyms:(1'R,2'R,3'S)-2-<2'-(2''-nitrophenylselanylmethyl)-3'-methylcyclopentyl>propan-2-ol

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Chemical Property of (1'R,2'R,3'S)-2-<2'-(2''-nitrophenylselanylmethyl)-3'-methylcyclopentyl>propan-2-ol

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Technology Process of (1'R,2'R,3'S)-2-<2'-(2''-nitrophenylselanylmethyl)-3'-methylcyclopentyl>propan-2-ol

There total 3 articles about (1'R,2'R,3'S)-2-<2'-(2''-nitrophenylselanylmethyl)-3'-methylcyclopentyl>propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 51694-22-5
ortho-nitrophenyl selenocyanate

: 162599-47-5
(1'R,2'R,3'S)-2-(2'-hydroxymethyl-3'-methylcyclopentyl)propan-2-ol

: 162460-45-9
(1'R,2'R,3'S)-2-<2'-(2''-nitrophenylselanylmethyl)-3'-methylcyclopentyl>propan-2-ol

Guidance literature:: With tributylphosphine; In tetrahydrofuran; for 2h; Ambient temperature;

Reference yield:

: 2005-60-9,2078-88-8,30165-19-6,35337-16-7,35337-17-8,122045-56-1,134452-55-4
(1R,2R,5S)-2-Isopropenyl-5-methyl-cyclopentanecarboxylic acid methyl ester

: 162460-45-9
(1'R,2'R,3'S)-2-<2'-(2''-nitrophenylselanylmethyl)-3'-methylcyclopentyl>propan-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: MCPBA, KHCO₃ / CH₂Cl₂ / 2 h / 0 °C

2: LiAlH₄ / tetrahydrofuran / 4 h / Ambient temperature

3: 100 percent / Bu₃P / tetrahydrofuran / 2 h / Ambient temperature

With lithium aluminium tetrahydride; tributylphosphine; potassium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: (1R,2S,5R)-2-Methyl-5-(2-methyl-oxiranyl)-cyclopentanecarboxylic acid methyl ester

: 162460-45-9
(1'R,2'R,3'S)-2-<2'-(2''-nitrophenylselanylmethyl)-3'-methylcyclopentyl>propan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran / 4 h / Ambient temperature

2: 100 percent / Bu₃P / tetrahydrofuran / 2 h / Ambient temperature

With lithium aluminium tetrahydride; tributylphosphine; In tetrahydrofuran;