tert-butyl (4-t-butylbenzoyl)oxycarbamate

Base Information

• Chemical Name: tert-butyl (4-t-butylbenzoyl)oxycarbamate
• CAS No.: 1613027-57-8
• Molecular Formula: C₁₆H₂₃NO₄
• Molecular Weight: 293.363
• Mol file: 1613027-57-8.mol

Synonyms:tert-butyl (4-t-butylbenzoyl)oxycarbamate

Chemical Property of tert-butyl (4-t-butylbenzoyl)oxycarbamate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of tert-butyl (4-t-butylbenzoyl)oxycarbamate

There total 1 articles about tert-butyl (4-t-butylbenzoyl)oxycarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-Butyl N-hydroxycarbamate (36016-38-3) + p-tert-butyl benzoyl chloride (1710-98-1) → tert-butyl (4-t-butylbenzoyl)oxycarbamate (1613027-57-8)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 25 ℃; Inert atmosphere;

DOI:10.1021/ol501338h

Reference yield: 22.0%

tert-butyl (4-t-butylbenzoyl)oxycarbamate (1613027-57-8) + S-methyl-S-phenylsulfoximine (4381-25-3) → S-[2-(tert-butoxycarbonyl)aminophenyl]-S-methylsulfoximine

Guidance literature:

With tris(acetonitrile)(η5-pentamethylcyclopentadienyl)rhodium(III) hexafluoroantimonate; sodium acetate; In 1,2-dichloro-ethane; at 100 ℃; for 12h; Inert atmosphere; Schlenk technique;

DOI:10.1002/chem.201602550

Reference yield:

2-phenylpyridine (1008-89-5) + tert-butyl (4-t-butylbenzoyl)oxycarbamate (1613027-57-8) → N-(tert-butyloxycarbonyl)-2-(pyridin-2-yl)aniline (1318768-17-0)

Guidance literature:

With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; silver(I) 4-methylbenzenesulfonate; In 1,2-dichloro-ethane; at 25 ℃; for 10h; Inert atmosphere;

DOI:10.1021/ol501338h

upstream raw materials:

tert-Butyl N-hydroxycarbamate

p-tert-butyl benzoyl chloride

Downstream raw materials:

N-(tert-butyloxycarbonyl)-2-(pyridin-2-yl)aniline