m-(pentafluorobenzyloxy)-E-3-methylcinnamoyl chloride

Base Information

Chemical Name:m-(pentafluorobenzyloxy)-E-3-methylcinnamoyl chloride
CAS No.:131693-35-1
Molecular Formula:C₁₇H₁₀ClF₅O₂
Molecular Weight:376.71
Hs Code.:

Synonyms:m-(pentafluorobenzyloxy)-E-3-methylcinnamoyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of m-(pentafluorobenzyloxy)-E-3-methylcinnamoyl chloride

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Technology Process of m-(pentafluorobenzyloxy)-E-3-methylcinnamoyl chloride

There total 6 articles about m-(pentafluorobenzyloxy)-E-3-methylcinnamoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 131693-36-2
m-pentafluorobenzyloxy-β-methyl-cinnamic acid

: 131693-35-1
m-(pentafluorobenzyloxy)-E-3-methylcinnamoyl chloride

Guidance literature:: With thionyl chloride; In benzene; at 90 ℃; for 20h;
DOI:10.1016/S0040-4020(01)87912-6

Reference yield:

: 121-71-1
3-Hydroxyacetophenone

: 131693-35-1
m-(pentafluorobenzyloxy)-E-3-methylcinnamoyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / aq.NaOH, tetra-n-butylammonium sulfate / CH₂Cl₂ / 3 h / Ambient temperature; similar yield with K₂CO₃ in acetone (reflux, 2 h)

2: 27 percent / xylene / 34 h / Heating

3: hydrolysis

4: 98 percent / SOCl₂ / benzene / 20 h / 90 °C

With sodium hydroxide; thionyl chloride; tetrabutylammonium sulfate; In dichloromethane; xylene; benzene;
DOI:10.1016/S0040-4020(01)87912-6

Reference yield:

: 131693-26-0
m-(pentafluorobenzyloxy)acetophenone

: 131693-35-1
m-(pentafluorobenzyloxy)-E-3-methylcinnamoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 27 percent / xylene / 34 h / Heating

2: hydrolysis

3: 98 percent / SOCl₂ / benzene / 20 h / 90 °C

With thionyl chloride; In xylene; benzene;
DOI:10.1016/S0040-4020(01)87912-6