C₄₅H₇₂BN₃O₁₀

Base Information

Chemical Name:C₄₅H₇₂BN₃O₁₀
CAS No.:1613270-30-6
Molecular Formula:C₄₅H₇₂BN₃O₁₀
Molecular Weight:825.892
Hs Code.:

C<sub>45</sub>H<sub>72</sub>BN<sub>3</sub>O<sub>10</sub>

Synonyms:C₄₅H₇₂BN₃O₁₀

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Chemical Property of C₄₅H₇₂BN₃O₁₀

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Technology Process of C₄₅H₇₂BN₃O₁₀

There total 30 articles about C₄₅H₇₂BN₃O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1256336-53-4
3-[(2R)-2-[bis(trimethylsilyl)amino]-2-[(3aS,4S,6S,7aR)-hexahydro-3a,5,5-trimethyl-4,6-methano-1,3,2-benzodioxaborol-2-yl]ethyl]-2-methoxy-benzoic acid 1,1-dimethylethyl ester

: 1613270-14-6
2-(trans-4-(2,2,12,12-tetramethyl-4,10-dioxo-3,11-dioxa-5,9-diazatridecan-6-yl)cyclohexyl)acetic acid

: 1613270-30-6
C₄₅H₇₂BN₃O₁₀

Guidance literature:: 2-(trans-4-(2,2,12,12-tetramethyl-4,10-dioxo-3,11-dioxa-5,9-diazatridecan-6-yl)cyclohexyl)acetic acid; With 4-methyl-morpholine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; N,N-dimethyl acetamide; at 20 ℃; for 1.5h; Inert atmosphere;

3-[(2R)-2-[bis(trimethylsilyl)amino]-2-[(3aS,4S,6S,7aR)-hexahydro-3a,5,5-trimethyl-4,6-methano-1,3,2-benzodioxaborol-2-yl]ethyl]-2-methoxy-benzoic acid 1,1-dimethylethyl ester; In tetrahydrofuran; N,N-dimethyl acetamide; at 20 ℃;

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 1613270-30-6
C₄₅H₇₂BN₃O₁₀

Guidance literature:: Multi-step reaction with 23 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

1.2: 3.17 h / 0 °C

2.1: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 1810.07 Torr

3.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.58 h / 0 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran; mineral oil / 1.17 h / 0 - 20 °C

4.2: 20 °C

5.1: hydrogenchloride / water; acetonitrile / 2 h / 20 °C

6.1: potassium tert-butylate / tetrahydrofuran / 2.5 h / -78 - 20 °C / Inert atmosphere

6.2: -40 - 20 °C

7.1: diborane-dimethylsulfide complex / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

7.2: 2.5 h / 0 - 20 °C

8.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

8.2: 0.58 h / -78 - 20 °C

9.1: titanium(IV) tetraethanolate / tetrahydrofuran / 20 h / 20 °C / Inert atmosphere

10.1: tetrahydrofuran; dichloromethane / 1 h / 0 °C / Inert atmosphere

11.1: hydrogenchloride / methanol; 1,4-dioxane / 0.5 h / 20 °C

12.1: triethylamine / dichloromethane / 4 h / 0 - 20 °C

13.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / 1,4-dioxane; water / 18 h / 20 °C

13.2: 4 h / 20 °C

14.1: palladium 10% on activated carbon; hydrogen / methanol / 20 °C

15.1: triethylamine; dmap / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

16.1: sodium tetrahydroborate; ethanol / 0.33 h / -10 - 0 °C

17.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

18.1: sodium azide / N,N-dimethyl-formamide / 80 °C

19.1: palladium 10% on activated carbon; hydrogen / methanol / 18 h / 20 °C

20.1: triethylamine / dichloromethane / 0 - 20 °C

21.1: potassium carbonate / methanol / 3 h / 20 °C

22.1: sodium periodate; rhodium(III) chloride hydrate / water; acetonitrile; tetrachloromethane / 2 h / 20 °C

23.1: 4-methyl-morpholine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / tetrahydrofuran; N,N-dimethyl acetamide / 1.5 h / 20 °C / Inert atmosphere

23.2: 20 °C

With 4-methyl-morpholine; hydrogenchloride; dmap; titanium(IV) tetraethanolate; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; lithium aluminium tetrahydride; sodium azide; oxalyl dichloride; ethanol; rhodium(III) chloride hydrate; diborane-dimethylsulfide complex; palladium 10% on activated carbon; potassium tert-butylate; hydrogen; sodium hydride; potassium carbonate; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; 1,4-dioxane; methanol; tetrachloromethane; diethyl ether; dichloromethane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; acetonitrile; mineral oil; 6.1: |Wittig Olefination / 6.2: |Wittig Olefination / 8.1: |Swern Oxidation / 8.2: |Swern Oxidation;

Reference yield:

: 18680-27-8
pinanediol

: 1613270-30-6
C₄₅H₇₂BN₃O₁₀

Guidance literature:: Multi-step reaction with 7 steps

1.1: toluene / 3 h

2.1: thionyl chloride / 1 h / 95 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.42 h / -5 °C

3.2: 4 h

4.1: n-butyllithium / tetrahydrofuran; hexane / 1.58 h / Cooling

4.2: 16.5 h

5.1: tetrahydrofuran / 0.5 h / -60 °C

5.2: 0.5 h / -60 °C

5.3: 1.5 h / -16 - 0 °C

6.1: tetrahydrofuran / 16.75 h / -78 °C

7.1: 4-methyl-morpholine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / tetrahydrofuran; N,N-dimethyl acetamide / 1.5 h / 20 °C / Inert atmosphere

7.2: 20 °C

With 4-methyl-morpholine; n-butyllithium; thionyl chloride; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; hexane; N,N-dimethyl acetamide; toluene;