3-[3-(boranatodiphenylphosphino)propylthio]-3',4,4'-trimethyl-tetrathiafulvalene

Base Information

Chemical Name:3-[3-(boranatodiphenylphosphino)propylthio]-3',4,4'-trimethyl-tetrathiafulvalene
CAS No.:507444-60-2
Molecular Formula:C₂₄H₂₈BPS₅
Molecular Weight:518.601
Hs Code.:

Synonyms:3-[3-(boranatodiphenylphosphino)propylthio]-3',4,4'-trimethyl-tetrathiafulvalene

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Chemical Property of 3-[3-(boranatodiphenylphosphino)propylthio]-3',4,4'-trimethyl-tetrathiafulvalene

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Technology Process of 3-[3-(boranatodiphenylphosphino)propylthio]-3',4,4'-trimethyl-tetrathiafulvalene

There total 1 articles about 3-[3-(boranatodiphenylphosphino)propylthio]-3',4,4'-trimethyl-tetrathiafulvalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: (3-chloropropyl)diphenylphosphine-borane

: 350503-25-2
3-[(4,4',5'-trimethyl-2,2'-bi-1,3-dithiolyliden-4-yl)thio]propanenitrile

: 507444-60-2
3-[3-(boranatodiphenylphosphino)propylthio]-3',4,4'-trimethyl-tetrathiafulvalene

Guidance literature:: With cesium hydroxide; In methanol; water; N,N-dimethyl-formamide; Ar; addn. of CsOH and H2O in methanol to DMF soln. of tetrathiafulvalenederivative, stirring at room temp. for 30 min, addn. of borane, stirrin g for 12 h; solvent evapn., extn. the residue with CH2Cl2, washing with water, drying the organic layer over Na2SO4, evapn., chromy. (silica gel, CH2Cl2/PE 4:1); elem. anal.;
DOI:10.1021/ic026186f

Reference yield: 81.0%

: 14515-95-8,56083-13-7
cis-(tungsten tetracarbonyl bipiperidine)

: 507444-60-2
3-[3-(boranatodiphenylphosphino)propylthio]-3',4,4'-trimethyl-tetrathiafulvalene

: 507444-64-6
cis-W(CO)4[P,S-3-[3-(diphenylphosphino)propylthio]-3,4,4'-tetrathiafulvalene]

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In toluene; Ar; addn. of DABCO to toluene soln. of ligand, stirring for 4 h at 50°C, addn. of Mo complex, in degassed CH2Cl2, stirring for 15 min; solvent removal, extn. the residue with CH2Cl2, washing with water, chromy. (silica gel, 4:1 CH2Cl2/PE);
DOI:10.1021/ic026186f

Reference yield: 20.0%

: 59967-36-1,65337-26-0
cis-tetracarbonylbis(piperidine)molybdenum

: 507444-60-2
3-[3-(boranatodiphenylphosphino)propylthio]-3',4,4'-trimethyl-tetrathiafulvalene

: 507444-62-4
cis-Mo(CO)4[3-[3-(diphenylphosphino)propylthio]-3,4,4'-tetrathiafulvalene]2

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In toluene; Ar; addn. of DABCO to toluene soln. of ligand, stirring for 4 h at 50°C, addn. of Mo complex, in degassed CH2Cl2, stirring for 15 min; solvent removal, extn. the residue with CH2Cl2, washing with water, chromy. (silica gel, 4:1 CH2Cl2/PE); elem. anal.;
DOI:10.1021/ic026186f