cis-W(CO)4[P,S-3-[3-(diphenylphosphino)propylthio]-3,4,4'-tetrathiafulvalene]

Base Information

Chemical Name:cis-W(CO)4[P,S-3-[3-(diphenylphosphino)propylthio]-3,4,4'-tetrathiafulvalene]
CAS No.:507444-64-6
Molecular Formula:C₂₈H₂₅O₄PS₅W
Molecular Weight:800.658
Hs Code.:

Synonyms:cis-W(CO)4[P,S-3-[3-(diphenylphosphino)propylthio]-3,4,4'-tetrathiafulvalene]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-W(CO)4[P,S-3-[3-(diphenylphosphino)propylthio]-3,4,4'-tetrathiafulvalene]

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Technology Process of cis-W(CO)4[P,S-3-[3-(diphenylphosphino)propylthio]-3,4,4'-tetrathiafulvalene]

There total 1 articles about cis-W(CO)4[P,S-3-[3-(diphenylphosphino)propylthio]-3,4,4'-tetrathiafulvalene] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 14515-95-8,56083-13-7
cis-(tungsten tetracarbonyl bipiperidine)

: 507444-60-2
3-[3-(boranatodiphenylphosphino)propylthio]-3',4,4'-trimethyl-tetrathiafulvalene

: 507444-64-6
cis-W(CO)4[P,S-3-[3-(diphenylphosphino)propylthio]-3,4,4'-tetrathiafulvalene]

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In toluene; Ar; addn. of DABCO to toluene soln. of ligand, stirring for 4 h at 50°C, addn. of Mo complex, in degassed CH2Cl2, stirring for 15 min; solvent removal, extn. the residue with CH2Cl2, washing with water, chromy. (silica gel, 4:1 CH2Cl2/PE);
DOI:10.1021/ic026186f