trans-4-<<<<(1R-trans)-3-<<<2-(phenylmethyl)-4-furyl>methoxy>carbonyl>-2,2-dimethyl-1-cyclopropyl>carbonyl>amino>methyl>cyclohexane-1-carboxylic acid

Base Information

Chemical Name:trans-4-<<<<(1R-trans)-3-<<<2-(phenylmethyl)-4-furyl>methoxy>carbonyl>-2,2-dimethyl-1-cyclopropyl>carbonyl>amino>methyl>cyclohexane-1-carboxylic acid
CAS No.:151059-60-8
Molecular Formula:C₂₇H₃₃NO₆
Molecular Weight:467.562
Hs Code.:

trans-4-<<<<(1R-trans)-3-<<<2-(phenylmethyl)-4-furyl>methoxy>carbonyl>-2,2-dimethyl-1-cyclopropyl>carbonyl>amino>methyl>cyclohexane-1-carboxylic acid

Synonyms:trans-4-<<<<(1R-trans)-3-<<<2-(phenylmethyl)-4-furyl>methoxy>carbonyl>-2,2-dimethyl-1-cyclopropyl>carbonyl>amino>methyl>cyclohexane-1-carboxylic acid

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Chemical Property of trans-4-<<<<(1R-trans)-3-<<<2-(phenylmethyl)-4-furyl>methoxy>carbonyl>-2,2-dimethyl-1-cyclopropyl>carbonyl>amino>methyl>cyclohexane-1-carboxylic acid

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Technology Process of trans-4-<<<<(1R-trans)-3-<<<2-(phenylmethyl)-4-furyl>methoxy>carbonyl>-2,2-dimethyl-1-cyclopropyl>carbonyl>amino>methyl>cyclohexane-1-carboxylic acid

There total 5 articles about trans-4-<<<<(1R-trans)-3-<<<2-(phenylmethyl)-4-furyl>methoxy>carbonyl>-2,2-dimethyl-1-cyclopropyl>carbonyl>amino>methyl>cyclohexane-1-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 151059-59-5
(1R-trans)-3-<<<<4-<<2-(trimethylsilyl)ethoxy>carbonyl>cyclohexyl>methyl>amino>carbonyl>-2,2-dimethylcyclopropane-1-carboxylic acid, <2-(phenylmethyl)-4-furyl>methyl ester

: 151059-60-8
trans-4-<<<<(1R-trans)-3-<<<2-(phenylmethyl)-4-furyl>methoxy>carbonyl>-2,2-dimethyl-1-cyclopropyl>carbonyl>amino>methyl>cyclohexane-1-carboxylic acid

Guidance literature:: With tetraethylammonium fluoride; In acetonitrile; at 20 ℃;
DOI:10.1021/jf00035a038

Reference yield:

: 20416-09-5
(5-benzylfuran-3-yl)methanol

: 151059-60-8
trans-4-<<<<(1R-trans)-3-<<<2-(phenylmethyl)-4-furyl>methoxy>carbonyl>-2,2-dimethyl-1-cyclopropyl>carbonyl>amino>methyl>cyclohexane-1-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 79 percent / 1,3-dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CH₂Cl₂ / 0 - 20 °C

2: 61 percent / tetraethylammonium fluoride / acetonitrile / 20 °C

3: 1.) 1,3-dicyclohexylcarbodiimide / 1.) CH₂Cl₂, 0 deg C, 20 min, 2.) CH₂Cl₂, RT, overnight

4: 97 percent / tetraethylammonium fluoride / acetonitrile / 20 °C

With dmap; tetraethylammonium fluoride; dicyclohexyl-carbodiimide; In dichloromethane; acetonitrile;
DOI:10.1021/jf00035a038

Reference yield:

: 151059-51-7
(1R-trans)-2,2-dimethylcyclopropane-1,3-dicarboxylic acid, 2-(trimethylsilyl)ethyl monoester

: 151059-60-8
trans-4-<<<<(1R-trans)-3-<<<2-(phenylmethyl)-4-furyl>methoxy>carbonyl>-2,2-dimethyl-1-cyclopropyl>carbonyl>amino>methyl>cyclohexane-1-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 79 percent / 1,3-dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CH₂Cl₂ / 0 - 20 °C

2: 61 percent / tetraethylammonium fluoride / acetonitrile / 20 °C

3: 1.) 1,3-dicyclohexylcarbodiimide / 1.) CH₂Cl₂, 0 deg C, 20 min, 2.) CH₂Cl₂, RT, overnight

4: 97 percent / tetraethylammonium fluoride / acetonitrile / 20 °C

With dmap; tetraethylammonium fluoride; dicyclohexyl-carbodiimide; In dichloromethane; acetonitrile;
DOI:10.1021/jf00035a038