Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (1R,2S,3R,4R,5S,6R)-2,3,5-tris-benzyloxy-4,6-bis-[(2-cyano-ethoxy)-diisopropylamino-phosphanyloxy]-cyclohexyl ester

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Chemical Name:Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (1R,2S,3R,4R,5S,6R)-2,3,5-tris-benzyloxy-4,6-bis-[(2-cyano-ethoxy)-diisopropylamino-phosphanyloxy]-cyclohexyl ester
CAS No.:109522-10-3
Molecular Formula:C₅₄H₈₁N₆O₉P₃
Molecular Weight:1051.19
Hs Code.:

Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (1R,2S,3R,4R,5S,6R)-2,3,5-tris-benzyloxy-4,6-bis-[(2-cyano-ethoxy)-diisopropylamino-phosphanyloxy]-cyclohexyl ester

Synonyms:Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (1R,2S,3R,4R,5S,6R)-2,3,5-tris-benzyloxy-4,6-bis-[(2-cyano-ethoxy)-diisopropylamino-phosphanyloxy]-cyclohexyl ester

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Chemical Property of Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (1R,2S,3R,4R,5S,6R)-2,3,5-tris-benzyloxy-4,6-bis-[(2-cyano-ethoxy)-diisopropylamino-phosphanyloxy]-cyclohexyl ester

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Technology Process of Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (1R,2S,3R,4R,5S,6R)-2,3,5-tris-benzyloxy-4,6-bis-[(2-cyano-ethoxy)-diisopropylamino-phosphanyloxy]-cyclohexyl ester

There total 1 articles about Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (1R,2S,3R,4R,5S,6R)-2,3,5-tris-benzyloxy-4,6-bis-[(2-cyano-ethoxy)-diisopropylamino-phosphanyloxy]-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 124482-92-4,89992-70-1
2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

: 98906-30-0,104873-76-9,111466-07-0,114297-88-0,114297-91-5,114419-08-8,115184-71-9,115509-75-6,115509-76-7,118354-54-4,118354-55-5,128163-34-8,129706-80-5,136521-84-1,149713-88-2,149713-95-1
(±)-2,3,6-tri-O-benzyl-myo-inositol

: 109522-10-3
Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (1R,2S,3R,4R,5S,6R)-2,3,5-tris-benzyloxy-4,6-bis-[(2-cyano-ethoxy)-diisopropylamino-phosphanyloxy]-cyclohexyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)96110-0

Reference yield:

: 109522-10-3
Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (1R,2S,3R,4R,5S,6R)-2,3,5-tris-benzyloxy-4,6-bis-[(2-cyano-ethoxy)-diisopropylamino-phosphanyloxy]-cyclohexyl ester

: DL-myo-inositol 1,4,5-triphosphate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrazole

2: 100 percent / t-butyl hydroperoxide

3: 50 percent / Na / liquid ammonia

With 1H-tetrazole; tert.-butylhydroperoxide; sodium; In ammonia;
DOI:10.1016/S0040-4039(00)96110-0