12-benzyl-3-(4-chloro-3-methoxyphenyl)-8-(phenylsulfonyl)-2-pyridin-4-yl-7,8,9,10-tetrahydro-6H-7,10-epiminocyclohepta[e]pyrazolo[1,5-a]pyrimidine

Base Information

Chemical Name:12-benzyl-3-(4-chloro-3-methoxyphenyl)-8-(phenylsulfonyl)-2-pyridin-4-yl-7,8,9,10-tetrahydro-6H-7,10-epiminocyclohepta[e]pyrazolo[1,5-a]pyrimidine
CAS No.:1184103-08-9
Molecular Formula:C₃₆H₃₀ClN₅O₃S
Molecular Weight:648.185
Hs Code.:

12-benzyl-3-(4-chloro-3-methoxyphenyl)-8-(phenylsulfonyl)-2-pyridin-4-yl-7,8,9,10-tetrahydro-6H-7,10-epiminocyclohepta[e]pyrazolo[1,5-a]pyrimidine

Synonyms:12-benzyl-3-(4-chloro-3-methoxyphenyl)-8-(phenylsulfonyl)-2-pyridin-4-yl-7,8,9,10-tetrahydro-6H-7,10-epiminocyclohepta[e]pyrazolo[1,5-a]pyrimidine

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Chemical Property of 12-benzyl-3-(4-chloro-3-methoxyphenyl)-8-(phenylsulfonyl)-2-pyridin-4-yl-7,8,9,10-tetrahydro-6H-7,10-epiminocyclohepta[e]pyrazolo[1,5-a]pyrimidine

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Technology Process of 12-benzyl-3-(4-chloro-3-methoxyphenyl)-8-(phenylsulfonyl)-2-pyridin-4-yl-7,8,9,10-tetrahydro-6H-7,10-epiminocyclohepta[e]pyrazolo[1,5-a]pyrimidine

There total 9 articles about 12-benzyl-3-(4-chloro-3-methoxyphenyl)-8-(phenylsulfonyl)-2-pyridin-4-yl-7,8,9,10-tetrahydro-6H-7,10-epiminocyclohepta[e]pyrazolo[1,5-a]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.2%

: 1134598-79-0
4-(4-chloro-3-methoxyphenyl)-5-pyridin-4-yl-1H-pyrazol-3-amine

: 1184103-60-3
8-benzyl-3-[(dimethylamino)methylene]-6-(phenylsulfonyl)-8-azabicyclo[3.2.1]octane-2-one

: 1184103-08-9
12-benzyl-3-(4-chloro-3-methoxyphenyl)-8-(phenylsulfonyl)-2-pyridin-4-yl-7,8,9,10-tetrahydro-6H-7,10-epiminocyclohepta[e]pyrazolo[1,5-a]pyrimidine

Guidance literature:: With acetic acid; at 100 ℃; for 19h;

Reference yield:

: 1087750-66-0
8-benzyl-6-(phenylsulfonyl)-8-azabicyclo[3.2.1]oct-3-en-2-one

: 1184103-08-9
12-benzyl-3-(4-chloro-3-methoxyphenyl)-8-(phenylsulfonyl)-2-pyridin-4-yl-7,8,9,10-tetrahydro-6H-7,10-epiminocyclohepta[e]pyrazolo[1,5-a]pyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / methanol; acetone / 20 h / 20 °C / 760.05 Torr

2: 7 h / 100 °C

3: acetic acid / 19 h / 100 °C

With hydrogen; acetic acid; palladium 10% on activated carbon; In methanol; acetone;

Reference yield:

: 54429-89-9
N-benzyl-3-oxypyridinium betaine

: 1184103-08-9
12-benzyl-3-(4-chloro-3-methoxyphenyl)-8-(phenylsulfonyl)-2-pyridin-4-yl-7,8,9,10-tetrahydro-6H-7,10-epiminocyclohepta[e]pyrazolo[1,5-a]pyrimidine

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 20 h / 95 °C

2: hydrogen / palladium 10% on activated carbon / methanol; acetone / 20 h / 20 °C / 760.05 Torr

3: 7 h / 100 °C

4: acetic acid / 19 h / 100 °C

With hydrogen; acetic acid; palladium 10% on activated carbon; In tetrahydrofuran; methanol; acetone;