2-(4-((pyridin-2-ylmethyl)amino)phenyl)benzo[d][1,3,2]dithiazole 1,1,3,3-tetraoxide hydrochloride

Base Information

Chemical Name:2-(4-((pyridin-2-ylmethyl)amino)phenyl)benzo[d][1,3,2]dithiazole 1,1,3,3-tetraoxide hydrochloride
CAS No.:1239013-74-1
Molecular Formula:C₁₈H₁₅N₃O₄S₂*ClH
Molecular Weight:437.928
Hs Code.:

Synonyms:2-(4-((pyridin-2-ylmethyl)amino)phenyl)benzo[d][1,3,2]dithiazole 1,1,3,3-tetraoxide hydrochloride

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Chemical Property of 2-(4-((pyridin-2-ylmethyl)amino)phenyl)benzo[d][1,3,2]dithiazole 1,1,3,3-tetraoxide hydrochloride

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Technology Process of 2-(4-((pyridin-2-ylmethyl)amino)phenyl)benzo[d][1,3,2]dithiazole 1,1,3,3-tetraoxide hydrochloride

There total 5 articles about 2-(4-((pyridin-2-ylmethyl)amino)phenyl)benzo[d][1,3,2]dithiazole 1,1,3,3-tetraoxide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1239013-94-5
tert-butyl N-(4-aminophenyl)-N-(pyridin-2-ylmethyl)carbamate

: 6461-76-3
1,2-benzenedisulfonyl dichloride

: 1239013-74-1
2-(4-((pyridin-2-ylmethyl)amino)phenyl)benzo[d][1,3,2]dithiazole 1,1,3,3-tetraoxide hydrochloride

Guidance literature:: tert-butyl N-(4-aminophenyl)-N-(pyridin-2-ylmethyl)carbamate; 1,2-benzenedisulfonyl dichloride; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In DCE; at 40 ℃; for 48h;

With hydrogenchloride; In 1,4-dioxane; dichloromethane; for 3h;

Reference yield:

: 408365-67-3
4-nitro-N-(pyridin-2-ylmethyl)aniline

: 1239013-74-1
2-(4-((pyridin-2-ylmethyl)amino)phenyl)benzo[d][1,3,2]dithiazole 1,1,3,3-tetraoxide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 6 h / Reflux

2.1: palladium on activated charcoal; hydrogen / methanol / 14 h

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 1,2-dichloro-ethane / 18 h / 40 °C

3.2: 3 h

With dmap; palladium on activated charcoal; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; 1,2-dichloro-ethane;
DOI:10.1021/jm200956q

Reference yield:

: 1239013-93-4
tert-butyl N-(4-nitrophenyl)-N-(pyridin-2-ylmethyl)carbamate

: 1239013-74-1
2-(4-((pyridin-2-ylmethyl)amino)phenyl)benzo[d][1,3,2]dithiazole 1,1,3,3-tetraoxide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: palladium on activated charcoal; hydrogen / methanol / 14 h

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 1,2-dichloro-ethane / 18 h / 40 °C

2.2: 3 h

With palladium on activated charcoal; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; 1,2-dichloro-ethane;
DOI:10.1021/jm200956q