methyl (2RS,3SR)-2-methyl-2-<(2'-methoxyethoxy)methoxy>-3-hydroxybenzenepropanoate

Base Information

Chemical Name:methyl (2RS,3SR)-2-methyl-2-<(2'-methoxyethoxy)methoxy>-3-hydroxybenzenepropanoate
CAS No.:92817-37-3
Molecular Formula:C₁₅H₂₂O₆
Molecular Weight:298.336
Hs Code.:

Synonyms:methyl (2RS,3SR)-2-methyl-2-<(2'-methoxyethoxy)methoxy>-3-hydroxybenzenepropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2RS,3SR)-2-methyl-2-<(2'-methoxyethoxy)methoxy>-3-hydroxybenzenepropanoate

Chemical Property:

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Technology Process of methyl (2RS,3SR)-2-methyl-2-<(2'-methoxyethoxy)methoxy>-3-hydroxybenzenepropanoate

There total 2 articles about methyl (2RS,3SR)-2-methyl-2-<(2'-methoxyethoxy)methoxy>-3-hydroxybenzenepropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-52-7
benzaldehyde

: 78957-58-1
methyl (RS)-2-<(2'-methoxyethoxy)methoxy>propanoate

: 92817-37-3
methyl (2RS,3SR)-2-methyl-2-<(2'-methoxyethoxy)methoxy>-3-hydroxybenzenepropanoate

: 92817-36-2
methyl (2RS,3RS)-2-methyl-2-<(2'-methoxyethoxy)methoxy>-3-hydroxybenzenepropanoate

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) THF, -78 deg C, 45 min, 2.) -78 deg C;
DOI:10.1021/ja00406a064

Reference yield:

: 97231-83-9
2-(2-Methoxy-ethoxymethoxy)-propionic acid ethyl ester

: 92817-37-3
methyl (2RS,3SR)-2-methyl-2-<(2'-methoxyethoxy)methoxy>-3-hydroxybenzenepropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃

2: 1.) LDA / 1.) THF, -78 deg C, 45 min, 2.) -78 deg C

With potassium carbonate; lithium diisopropyl amide;
DOI:10.1021/ja00406a064