(+/-)-3-[(2,3-dihydro-1H-inden-2-yl)oxy]-4-methoxy-α-[(trimethylsilyl)oxy]benzeneacetonitrile

Base Information

• Chemical Name: (+/-)-3-[(2,3-dihydro-1H-inden-2-yl)oxy]-4-methoxy-α-[(trimethylsilyl)oxy]benzeneacetonitrile
• CAS No.: 205699-63-4
• Molecular Formula: C₂₁H₂₅NO₃Si
• Molecular Weight: 367.52

Synonyms:(+/-)-3-[(2,3-dihydro-1H-inden-2-yl)oxy]-4-methoxy-α-[(trimethylsilyl)oxy]benzeneacetonitrile

Chemical Property of (+/-)-3-[(2,3-dihydro-1H-inden-2-yl)oxy]-4-methoxy-α-[(trimethylsilyl)oxy]benzeneacetonitrile

Chemical Property:

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Technology Process of (+/-)-3-[(2,3-dihydro-1H-inden-2-yl)oxy]-4-methoxy-α-[(trimethylsilyl)oxy]benzeneacetonitrile

There total 1 articles about (+/-)-3-[(2,3-dihydro-1H-inden-2-yl)oxy]-4-methoxy-α-[(trimethylsilyl)oxy]benzeneacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trimethylsilyl cyanide (7677-24-9) + 3-[(2,3-dihydro-1H-inden-2-yl)oxy]-4-methoxy-benzaldehyde (115898-38-9) → (+/-)-3-[(2,3-dihydro-1H-inden-2-yl)oxy]-4-methoxy-α-[(trimethylsilyl)oxy]benzeneacetonitrile (205699-63-4)

Guidance literature:

With zinc(II) iodide; In dichloromethane; at 20 ℃;

DOI:10.1016/S0960-894X(01)00817-4

Reference yield:

3,4-dihydro-2H-pyran (110-87-2) + toluene-4-sulfonic acid (104-15-4) + (+/-)-3-[(2,3-dihydro-1H-inden-2-yl)oxy]-4-methoxy-α-[(trimethylsilyl)oxy]benzeneacetonitrile (205699-63-4) → (+/-)-3-[(2,3-dihydro-1H-inden-2-yl)oxy]-4-methoxy-α-[(tetrahydro-2H-pyran-2-yl)oxy]benzeneacetonitrile

Guidance literature:

With hydrogenchloride; In methanol; dichloromethane;

Reference yield:

(+/-)-3-[(2,3-dihydro-1H-inden-2-yl)oxy]-4-methoxy-α-[(trimethylsilyl)oxy]benzeneacetonitrile (205699-63-4) → 2-[3-(indan-2-yloxy)-4-methoxy-phenyl]-2-trimethylsilanyloxy-ethylamine

Guidance literature:

With ammonia; hydrogen; nickel; In methanol;

DOI:10.1016/S0960-894X(01)00817-4

upstream raw materials:

trimethylsilyl cyanide

3-[(2,3-dihydro-1H-inden-2-yl)oxy]-4-methoxy-benzaldehyde

Downstream raw materials:

1-{2-hydroxy-2-[3-(indan-2-yloxy)-4-methoxy-phenyl]-ethyl}-1,3-dihydro-imidazol-2-one

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