N-{1-[[5-methyl-3-(2-methylsulfonylphenylsulfonyloxy)phenoxy]methyl]cyclopropylmethoxy}phthalimide

Base Information

• Chemical Name: N-{1-[[5-methyl-3-(2-methylsulfonylphenylsulfonyloxy)phenoxy]methyl]cyclopropylmethoxy}phthalimide
• CAS No.: 208642-97-1
• Molecular Formula: C₂₇H₂₅NO₉S₂
• Molecular Weight: 571.629

Synonyms:N-{1-[[5-methyl-3-(2-methylsulfonylphenylsulfonyloxy)phenoxy]methyl]cyclopropylmethoxy}phthalimide

Chemical Property of N-{1-[[5-methyl-3-(2-methylsulfonylphenylsulfonyloxy)phenoxy]methyl]cyclopropylmethoxy}phthalimide

Chemical Property:

Purity/Quality:

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Technology Process of N-{1-[[5-methyl-3-(2-methylsulfonylphenylsulfonyloxy)phenoxy]methyl]cyclopropylmethoxy}phthalimide

There total 5 articles about N-{1-[[5-methyl-3-(2-methylsulfonylphenylsulfonyloxy)phenoxy]methyl]cyclopropylmethoxy}phthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

N-hydroxyphthalimide (524-38-9) + [1-[5-methyl-3-(2-methylsulfonylphenylsulfonyloxy)phenoxy]methyl]cyclopropylmethanol + diethylazodicarboxylate (1972-28-7,218603-74-8) → N-{1-[[5-methyl-3-(2-methylsulfonylphenylsulfonyloxy)phenoxy]methyl]cyclopropylmethoxy}phthalimide (208642-97-1)

Guidance literature:

With triphenylphosphine; In tetrahydrofuran; ethyl acetate;

Reference yield:

3-hydroxy-5-methylphenyl 2-(methylsulfonyl)benzenesulfonate (197960-66-0) → N-{1-[[5-methyl-3-(2-methylsulfonylphenylsulfonyloxy)phenoxy]methyl]cyclopropylmethoxy}phthalimide (208642-97-1)

Guidance literature:

Multi-step reaction with 2 steps

1: TBP; ADDP / tetrahydrofuran

2: TPP; DEAD / tetrahydrofuran

With bithionol; thiamine diphosphate; 1,1'-azodicarbonyl-dipiperidine; diethylazodicarboxylate; In tetrahydrofuran; 1: Mitsunobu reaction / 2: Mitsunobu reaction;

DOI:10.1016/S0960-894X(03)00125-2

Reference yield:

[1-(hydroxymethyl)cyclopropyl]methanol (39590-81-3) → N-{1-[[5-methyl-3-(2-methylsulfonylphenylsulfonyloxy)phenoxy]methyl]cyclopropylmethoxy}phthalimide (208642-97-1)

Guidance literature:

Multi-step reaction with 2 steps

1: TBP; ADDP / tetrahydrofuran

2: TPP; DEAD / tetrahydrofuran

With bithionol; thiamine diphosphate; 1,1'-azodicarbonyl-dipiperidine; diethylazodicarboxylate; In tetrahydrofuran; 1: Mitsunobu reaction / 2: Mitsunobu reaction;

DOI:10.1016/S0960-894X(03)00125-2

upstream raw materials:

N-hydroxyphthalimide

2-methanesulfonyl-benzenesulfonic acid 3-(1-hydroxymethyl-cyclopropylmethoxy)-5-methyl-phenyl ester

[1-(hydroxymethyl)cyclopropyl]methanol

1-(bromomethyl)-1-(hydroxymethyl)cyclopropane

Downstream raw materials:

N-{1-[[5-methyl-3-(2-methylsulfonylphenylsulfonyloxy)phenoxy]methyl]cyclopropylmethoxy}amine

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