(S)-2-(4-(N-Boc-aminomethyl)benzoylamino)-5-((1-methylpyrrole-2-ylmethyl)amino)valerate 1-naphthalenemethylamide

Base Information

Chemical Name:(S)-2-(4-(N-Boc-aminomethyl)benzoylamino)-5-((1-methylpyrrole-2-ylmethyl)amino)valerate 1-naphthalenemethylamide
CAS No.:369655-43-6
Molecular Formula:C₃₅H₄₃N₅O₄
Molecular Weight:597.758
Hs Code.:

Synonyms:(S)-2-(4-(N-Boc-aminomethyl)benzoylamino)-5-((1-methylpyrrole-2-ylmethyl)amino)valerate 1-naphthalenemethylamide

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Chemical Property of (S)-2-(4-(N-Boc-aminomethyl)benzoylamino)-5-((1-methylpyrrole-2-ylmethyl)amino)valerate 1-naphthalenemethylamide

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Technology Process of (S)-2-(4-(N-Boc-aminomethyl)benzoylamino)-5-((1-methylpyrrole-2-ylmethyl)amino)valerate 1-naphthalenemethylamide

There total 1 articles about (S)-2-(4-(N-Boc-aminomethyl)benzoylamino)-5-((1-methylpyrrole-2-ylmethyl)amino)valerate 1-naphthalenemethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1192-58-1
N-methylpyrrole aldehyde

: 370594-24-4
Nα-4-(N-Boc-aminomethyl) benzoyl-Nδ-Cbz-L-ornithine 1-naphthalenemethylamide

: 369655-43-6
(S)-2-(4-(N-Boc-aminomethyl)benzoylamino)-5-((1-methylpyrrole-2-ylmethyl)amino)valerate 1-naphthalenemethylamide

Guidance literature:: Nα-4-(N-Boc-aminomethyl) benzoyl-Nδ-Cbz-L-ornithine 1-naphthalenemethylamide; With hydrogen; palladium 10% on activated carbon; In methanol; for 2.33333h; under 760.051 Torr;

N-methylpyrrole aldehyde; With sodium cyanoborohydride; acetic acid; at 20 ℃; for 25h; pH=5;

Reference yield:

: 369655-43-6
(S)-2-(4-(N-Boc-aminomethyl)benzoylamino)-5-((1-methylpyrrole-2-ylmethyl)amino)valerate 1-naphthalenemethylamide

: 13750-81-7
N-methyl-2-imidazolcarboxaldehyde

: (S)-2-(4-((1-methylimidazol-2-ylmethyl)aminomethyl)benzoylamino)-5-((1-methylpyrrol-2-ylmethyl)amino)valerate 1-naphthalenemethylamide hydrochloride

Guidance literature:: (S)-2-(4-(N-Boc-aminomethyl)benzoylamino)-5-((1-methylpyrrole-2-ylmethyl)amino)valerate 1-naphthalenemethylamide; With hydrogenchloride; In 1,4-dioxane; methanol; at 20 ℃; for 2h;

N-methyl-2-imidazolcarboxaldehyde; With triethylamine; In methanol; at 20 ℃; for 3h;

With hydrogenchloride; sodium tetrahydroborate; more than 3 stages;

Reference yield:

: 10200-59-6
Thiazole-2-carbaldehyde

: 369655-43-6
(S)-2-(4-(N-Boc-aminomethyl)benzoylamino)-5-((1-methylpyrrole-2-ylmethyl)amino)valerate 1-naphthalenemethylamide

: (S)-2-(4-((thiazol-2-ylmethyl) aminomethyl)benzoylamino)-5-((1-methylpyrrol-2-ylmethyl) amino) valerate 1-naphthalene methylamide hydrochloride

Guidance literature:: (S)-2-(4-(N-Boc-aminomethyl)benzoylamino)-5-((1-methylpyrrole-2-ylmethyl)amino)valerate 1-naphthalenemethylamide; With hydrogenchloride; In 1,4-dioxane; methanol; at 20 ℃; for 12h;

Thiazole-2-carbaldehyde; With triethylamine; In methanol; at 20 ℃; for 2.5h;

With hydrogenchloride; sodium tetrahydroborate; more than 3 stages;