N'-[3-bromo-2-cyano-5-[[dimethyl(oxo)-λ⁶-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine

Base Information

• Chemical Name: N'-[3-bromo-2-cyano-5-[[dimethyl(oxo)-λ⁶-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine
• CAS No.: 1609962-91-5
• Molecular Formula: C₁₂H₁₅BrN₄OS
• Molecular Weight: 343.247

Synonyms:N'-[3-bromo-2-cyano-5-[[dimethyl(oxo)-λ⁶-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine

Chemical Property of N'-[3-bromo-2-cyano-5-[[dimethyl(oxo)-λ⁶-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine

Chemical Property:

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Technology Process of N'-[3-bromo-2-cyano-5-[[dimethyl(oxo)-λ⁶-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine

There total 1 articles about N'-[3-bromo-2-cyano-5-[[dimethyl(oxo)-λ⁶-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ N'-[3-bromo-2-cyano-5-[[dimethyl(oxo)-λ6-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine (1609962-91-5)

Guidance literature:

With bis(1,5-cyclooctadiene)diiridium(I) dichloride; bis(pinacol)diborane; 4,4'-di-tert-butyl-2,2'-bipyridine; In n-heptane; for 48h; Reflux;

With copper diacetate; In methanol; at 20 ℃;

Reference yield: 79.0%

N'-[3-bromo-2-cyano-5-[[dimethyl(oxo)-λ6-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine (1609962-91-5) + cyclopropylboronic acid (411235-57-9) → N'-[2-cyano-3-cyclopropyl-5-[[dimethyl(oxo)-λ6-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine (1609962-95-9)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In 1,4-dioxane; at 80 ℃;

Reference yield: 71.0%

azetidine (503-29-7) + N'-[3-bromo-2-cyano-5-[[dimethyl(oxo)-λ6-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine (1609962-91-5) → N'-[3-(azetidin-1-yl)-2-cyano-5-[[dimethyl(oxo)-λ6-sulfanylidene]amino]phenyl]-N,N-dimethylformamidine

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; for 6h; Reflux;

Downstream raw materials:

C₂₃H₂₅FN₄O₃S

C₂₃H₂₆FN₅O₃S

N'-[2-cyano-3-cyclopropyl-5-[[dimethyl(oxo)-λ⁶-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine

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