(2S,3S)-3-[(1-oxo-2-cyclohexen-3-yl)amino]-2-(tert-butyldimethylsilyloxy)butyl bromide

Base Information

Chemical Name:(2S,3S)-3-[(1-oxo-2-cyclohexen-3-yl)amino]-2-(tert-butyldimethylsilyloxy)butyl bromide
CAS No.:782498-13-9
Molecular Formula:C₁₆H₃₀BrNO₂Si
Molecular Weight:376.409
Hs Code.:

Synonyms:(2S,3S)-3-[(1-oxo-2-cyclohexen-3-yl)amino]-2-(tert-butyldimethylsilyloxy)butyl bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-3-[(1-oxo-2-cyclohexen-3-yl)amino]-2-(tert-butyldimethylsilyloxy)butyl bromide

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Technology Process of (2S,3S)-3-[(1-oxo-2-cyclohexen-3-yl)amino]-2-(tert-butyldimethylsilyloxy)butyl bromide

There total 3 articles about (2S,3S)-3-[(1-oxo-2-cyclohexen-3-yl)amino]-2-(tert-butyldimethylsilyloxy)butyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 782498-12-8
(2S,3S)-3-[(tert-butoxycarbonyl)amino]-2-(tert-butyldimethylsilyloxy)butyl bromide

: 782498-13-9
(2S,3S)-3-[(1-oxo-2-cyclohexen-3-yl)amino]-2-(tert-butyldimethylsilyloxy)butyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: formic acid / CH₂Cl₂ / 4 h / 20 °C

2: 2.4 g / benzene / 4 h / Heating

With formic acid; In dichloromethane; benzene;
DOI:10.1002/anie.200460128 DOI:10.1021/jo061070c

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 782498-13-9
(2S,3S)-3-[(1-oxo-2-cyclohexen-3-yl)amino]-2-(tert-butyldimethylsilyloxy)butyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / imidazole / dimethylformamide / 20 h / 20 °C

2: formic acid / CH₂Cl₂ / 4 h / 20 °C

3: 2.4 g / benzene / 4 h / Heating

With 1H-imidazole; formic acid; In dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1002/anie.200460128