(3-Phenyl-propyl)-propyl-[3-(toluene-4-sulfonyl)-6,7,8,9-tetrahydro-3H-benzo[e]indol-8-yl]-amine

Base Information

• Chemical Name: (3-Phenyl-propyl)-propyl-[3-(toluene-4-sulfonyl)-6,7,8,9-tetrahydro-3H-benzo[e]indol-8-yl]-amine
• CAS No.: 163561-97-5
• Molecular Formula: C₃₁H₃₆N₂O₂S
• Molecular Weight: 500.705

Synonyms:(3-Phenyl-propyl)-propyl-[3-(toluene-4-sulfonyl)-6,7,8,9-tetrahydro-3H-benzo[e]indol-8-yl]-amine

Chemical Property of (3-Phenyl-propyl)-propyl-[3-(toluene-4-sulfonyl)-6,7,8,9-tetrahydro-3H-benzo[e]indol-8-yl]-amine

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Technology Process of (3-Phenyl-propyl)-propyl-[3-(toluene-4-sulfonyl)-6,7,8,9-tetrahydro-3H-benzo[e]indol-8-yl]-amine

There total 2 articles about (3-Phenyl-propyl)-propyl-[3-(toluene-4-sulfonyl)-6,7,8,9-tetrahydro-3H-benzo[e]indol-8-yl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-Bromo-3-phenylpropane (637-59-2) + Propyl-[3-(toluene-4-sulfonyl)-6,7,8,9-tetrahydro-3H-benzo[e]indol-8-yl]-amine (851727-83-8) → (3-Phenyl-propyl)-propyl-[3-(toluene-4-sulfonyl)-6,7,8,9-tetrahydro-3H-benzo[e]indol-8-yl]-amine (163561-97-5)

Guidance literature:

With sodium carbonate; In acetonitrile; Heating;

DOI:10.1021/jm00012a022

Reference yield:

3-(p-toluenesulfonyl)-6,7,8,9-tetrahydro-3H-benzindol-8-one (155591-01-8) → (3-Phenyl-propyl)-propyl-[3-(toluene-4-sulfonyl)-6,7,8,9-tetrahydro-3H-benzo[e]indol-8-yl]-amine (163561-97-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) p-toluenesulfonic acid, 2.) NaCNBH₃ / 1.) toluene, reflux, overnight, 2.) THF, CH₃OH, RT, overnight

2: 95 percent / Na₂CO₃ / acetonitrile / Heating

With sodium cyanoborohydride; sodium carbonate; toluene-4-sulfonic acid; In acetonitrile;

DOI:10.1021/jm00012a022

Reference yield: 90.0%

(3-Phenyl-propyl)-propyl-[3-(toluene-4-sulfonyl)-6,7,8,9-tetrahydro-3H-benzo[e]indol-8-yl]-amine (163561-97-5) → (3-Phenyl-propyl)-propyl-(6,7,8,9-tetrahydro-3H-benzo[e]indol-8-yl)-amine (163561-98-6)

Guidance literature:

With sodium methylate; In tetrahydrofuran; methanol; Heating;

DOI:10.1021/jm00012a022

upstream raw materials:

1-Bromo-3-phenylpropane

Propyl-[3-(toluene-4-sulfonyl)-6,7,8,9-tetrahydro-3H-benzo[e]indol-8-yl]-amine

3-(p-toluenesulfonyl)-6,7,8,9-tetrahydro-3H-benzindol-8-one

Downstream raw materials:

(3-Phenyl-propyl)-propyl-(6,7,8,9-tetrahydro-3H-benzo[e]indol-8-yl)-amine

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