2,2'-{[(4S,5S)-2,2-dimethyl-1,3-dioxolane-4,5-diyl]bis[methylene(benzylimino)]}diethanol

Base Information

Chemical Name:2,2'-{[(4S,5S)-2,2-dimethyl-1,3-dioxolane-4,5-diyl]bis[methylene(benzylimino)]}diethanol
CAS No.:934021-51-9
Molecular Formula:C₂₅H₃₆N₂O₄
Molecular Weight:428.572
Hs Code.:

Synonyms:2,2'-{[(4S,5S)-2,2-dimethyl-1,3-dioxolane-4,5-diyl]bis[methylene(benzylimino)]}diethanol

Suppliers and Price of 2,2'-{[(4S,5S)-2,2-dimethyl-1,3-dioxolane-4,5-diyl]bis[methylene(benzylimino)]}diethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,2'-{[(4S,5S)-2,2-dimethyl-1,3-dioxolane-4,5-diyl]bis[methylene(benzylimino)]}diethanol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,2'-{[(4S,5S)-2,2-dimethyl-1,3-dioxolane-4,5-diyl]bis[methylene(benzylimino)]}diethanol

There total 3 articles about 2,2'-{[(4S,5S)-2,2-dimethyl-1,3-dioxolane-4,5-diyl]bis[methylene(benzylimino)]}diethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 934021-50-8
2,2'-{[(4S,5S)-2,2-dimethyl-1,3-dioxolane-4,5-diyl]bis(methyleneimino)}diethanol

: 100-39-0
benzyl bromide

: 934021-51-9
2,2'-{[(4S,5S)-2,2-dimethyl-1,3-dioxolane-4,5-diyl]bis[methylene(benzylimino)]}diethanol

Guidance literature:: With potassium carbonate; In methanol; at 40 ℃; for 6h;
DOI:10.1016/j.tetasy.2007.01.004

Reference yield:

: 37031-29-1
(-)-dimethy-2,3-O-isopropylidene-L-tartrate

: 934021-51-9
2,2'-{[(4S,5S)-2,2-dimethyl-1,3-dioxolane-4,5-diyl]bis[methylene(benzylimino)]}diethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / NaCN / methanol / 20 h / 55 °C

2: 82 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

3: 93 percent / K₂CO₃ / methanol / 6 h / 40 °C

With lithium aluminium tetrahydride; sodium cyanide; potassium carbonate; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetasy.2007.01.004

Reference yield:

: 182749-20-8
(4R,5R)-N,N'-bis(2-hydroxyethyl)-2,2-dimethyl-1,3-dioxolane-4,5-dicarboxamide

: 934021-51-9
2,2'-{[(4S,5S)-2,2-dimethyl-1,3-dioxolane-4,5-diyl]bis[methylene(benzylimino)]}diethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

2: 93 percent / K₂CO₃ / methanol / 6 h / 40 °C

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetasy.2007.01.004