methyl (2-trifluoroacetamidoethyl 2,4-di-O-benzoyl-3-O-sulfo-β-D-glucopyranosid)uronate sodium salt

Base Information

Chemical Name:methyl (2-trifluoroacetamidoethyl 2,4-di-O-benzoyl-3-O-sulfo-β-D-glucopyranosid)uronate sodium salt
CAS No.:1352813-99-0
Molecular Formula:C₂₅H₂₃F₃NO₁₃S*Na
Molecular Weight:657.507
Hs Code.:

Synonyms:methyl (2-trifluoroacetamidoethyl 2,4-di-O-benzoyl-3-O-sulfo-β-D-glucopyranosid)uronate sodium salt

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Chemical Property of methyl (2-trifluoroacetamidoethyl 2,4-di-O-benzoyl-3-O-sulfo-β-D-glucopyranosid)uronate sodium salt

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Technology Process of methyl (2-trifluoroacetamidoethyl 2,4-di-O-benzoyl-3-O-sulfo-β-D-glucopyranosid)uronate sodium salt

There total 3 articles about methyl (2-trifluoroacetamidoethyl 2,4-di-O-benzoyl-3-O-sulfo-β-D-glucopyranosid)uronate sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1352813-98-9
methyl (2-trifluoroacetamidoethyl 2,4-di-O-benzoyl-β-D-glucopyranosid)uronate

: 1352813-99-0
methyl (2-trifluoroacetamidoethyl 2,4-di-O-benzoyl-3-O-sulfo-β-D-glucopyranosid)uronate sodium salt

Guidance literature:: methyl (2-trifluoroacetamidoethyl 2,4-di-O-benzoyl-β-D-glucopyranosid)uronate; With pyridine; sulfur trioxide pyridine complex; at 20 ℃; for 4h;

In methanol; for 0.5h;
DOI:10.1021/ja2083015

Reference yield:

: 1352813-97-8
methyl (2-trifluoroacetamidoethyl 3-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosid)uronate

: 1352813-99-0
methyl (2-trifluoroacetamidoethyl 2,4-di-O-benzoyl-3-O-sulfo-β-D-glucopyranosid)uronate sodium salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / methanol / 30 h / 20 °C

2.1: pyridine; sulfur trioxide pyridine complex / 4 h / 20 °C

2.2: Amberlite IRA-120 Na⁺ resin / 0.5 h

With pyridine; hydrogenchloride; sulfur trioxide pyridine complex; In methanol;
DOI:10.1021/ja2083015

Reference yield:

: methyl (3-O-acetyl-2,4-di-O-benzoyl-α-D-glucopyranosyl trichloroacetamidate)uronate

: 1352813-99-0
methyl (2-trifluoroacetamidoethyl 2,4-di-O-benzoyl-3-O-sulfo-β-D-glucopyranosid)uronate sodium salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 2 h

2.1: hydrogenchloride / methanol / 30 h / 20 °C

3.1: pyridine; sulfur trioxide pyridine complex / 4 h / 20 °C

3.2: Amberlite IRA-120 Na⁺ resin / 0.5 h

With pyridine; hydrogenchloride; boron trifluoride diethyl etherate; sulfur trioxide pyridine complex; In methanol; dichloromethane;
DOI:10.1021/ja2083015