Technology Process of 4',5-di-O-benzoylnaringenin 7-O-[methyl (2'',3'',4''-tri-O-acetyl)-β-D-glucopyranosyl uronate]
There total 3 articles about 4',5-di-O-benzoylnaringenin 7-O-[methyl (2'',3'',4''-tri-O-acetyl)-β-D-glucopyranosyl uronate] which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
dichloromethane;
at 20 ℃;
Molecular sieve;
Inert atmosphere;
Cooling with ice;
DOI:10.1021/jf1010403
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1H-imidazole; thiophenol / 1-methyl-pyrrolidin-2-one / 0 - 20 °C
2: boron trifluoride diethyl etherate / dichloromethane / 20 °C / Molecular sieve; Inert atmosphere; Cooling with ice
With
1H-imidazole; boron trifluoride diethyl etherate; thiophenol;
In
1-methyl-pyrrolidin-2-one; dichloromethane;
DOI:10.1021/jf1010403
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / tetrahydrofuran / 20 °C / Cooling with ice
2: 1H-imidazole; thiophenol / 1-methyl-pyrrolidin-2-one / 0 - 20 °C
3: boron trifluoride diethyl etherate / dichloromethane / 20 °C / Molecular sieve; Inert atmosphere; Cooling with ice
With
1H-imidazole; boron trifluoride diethyl etherate; thiophenol; triethylamine;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane;
DOI:10.1021/jf1010403
