C₃₂H₃₆N₂O₄

Base Information

• Chemical Name: C₃₂H₃₆N₂O₄
• CAS No.: 1353639-22-1
• Molecular Formula: C₃₂H₃₆N₂O₄
• Molecular Weight: 512.649
• Mol file: 1353639-22-1.mol

Synonyms:C₃₂H₃₆N₂O₄

Chemical Property of C₃₂H₃₆N₂O₄

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₃₂H₃₆N₂O₄

There total 5 articles about C₃₂H₃₆N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

ethyl 5-bromovalerate (14660-52-7) + C25H24N2O2 (552854-22-5) → C32H36N2O4 (1353639-22-1)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In butanone;

DOI:10.1021/ma202051c

Reference yield:

C32H30N2O2 (1353639-21-0) → C32H36N2O4 (1353639-22-1)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride; acetic acid

2: 18-crown-6 ether; potassium carbonate / butanone

With hydrogenchloride; 18-crown-6 ether; potassium carbonate; acetic acid; In butanone;

DOI:10.1021/ma202051c

Reference yield:

4-benzyloxybenzonitrile (52805-36-4) → C32H36N2O4 (1353639-22-1)

Guidance literature:

Multi-step reaction with 4 steps

1: hydroxylamine hydrochloride; sodium carbonate / ethanol

2: pyridine

3: hydrogenchloride; acetic acid

4: 18-crown-6 ether; potassium carbonate / butanone

With pyridine; hydrogenchloride; 18-crown-6 ether; hydroxylamine hydrochloride; sodium carbonate; potassium carbonate; acetic acid; In ethanol; butanone;

DOI:10.1021/ma202051c

upstream raw materials:

C₃₂H₃₀N₂O₂

ethyl 5-bromovalerate

C₂₅H₂₄N₂O₂

4-benzyloxybenzonitrile

Downstream raw materials:

C₃₀H₃₂N₂O₄