2-(2,4,6-Trichlor-phenylazo)-5-phenyl-pyrrol-3-carbonsaeuremethylester

Base Information

Chemical Name:2-(2,4,6-Trichlor-phenylazo)-5-phenyl-pyrrol-3-carbonsaeuremethylester
CAS No.:130256-12-1
Molecular Formula:C₁₈H₁₂Cl₃N₃O₂
Molecular Weight:408.671
Hs Code.:

Synonyms:2-(2,4,6-Trichlor-phenylazo)-5-phenyl-pyrrol-3-carbonsaeuremethylester

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Chemical Property of 2-(2,4,6-Trichlor-phenylazo)-5-phenyl-pyrrol-3-carbonsaeuremethylester

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Technology Process of 2-(2,4,6-Trichlor-phenylazo)-5-phenyl-pyrrol-3-carbonsaeuremethylester

There total 1 articles about 2-(2,4,6-Trichlor-phenylazo)-5-phenyl-pyrrol-3-carbonsaeuremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 104891-98-7,148637-76-7
Methyl 3-amino-3-(2,4,6-trichlorophenylazo)propenoate

: 70-11-1
α-bromoacetophenone

: 130256-12-1
2-(2,4,6-Trichlor-phenylazo)-5-phenyl-pyrrol-3-carbonsaeuremethylester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; for 0.5h; Ambient temperature; other α-halogenocarbonyl compounds;

Reference yield: 76.0%

: 130256-12-1
2-(2,4,6-Trichlor-phenylazo)-5-phenyl-pyrrol-3-carbonsaeuremethylester

: 130256-15-4
2-(2,4,6-Trichlor-phenylazo)-5-phenyl-pyrrol-3-carbonsaeurehydrazid

Guidance literature:: With hydrazine hydrate; In methanol; for 168h; Ambient temperature;

Reference yield:

: 130256-12-1
2-(2,4,6-Trichlor-phenylazo)-5-phenyl-pyrrol-3-carbonsaeuremethylester

: 130256-17-6
6-(2,4,6-Trichlorphenyl)-2-phenyl-5,6-dihydro-1H-pyrrolo<3.2-e><1,2,4>-triazin-5-on

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / 80percent N₂H₄*H₂O / methanol / 168 h / Ambient temperature

2: 82 percent / Isoamyl nitrite, conc. HCl / methanol / 0.08 h

3: 78 percent / toluene / 0.08 h / Heating

With hydrogenchloride; hydrazine hydrate; isopentyl nitrite; In methanol; toluene;