1-phenyl-2,3,4,5-tetra-p-tolylborole

Base Information

Chemical Name:1-phenyl-2,3,4,5-tetra-p-tolylborole
CAS No.:99643-61-5
Molecular Formula:C₃₈H₃₃B
Molecular Weight:500.491
Hs Code.:

Synonyms:1-phenyl-2,3,4,5-tetra-p-tolylborole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenyl-2,3,4,5-tetra-p-tolylborole

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Technology Process of 1-phenyl-2,3,4,5-tetra-p-tolylborole

There total 3 articles about 1-phenyl-2,3,4,5-tetra-p-tolylborole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 873-51-8
phenylborondichloride

: 99643-59-1
1,1-dimethyl-2,3,4,5-tetra(p-tolyl)stannole

: 753-73-1
dimethyltin dichloride

: 99643-61-5
1-phenyl-2,3,4,5-tetra-p-tolylborole

Guidance literature:: In tetrachloromethane; under Ar or N2, soln. of (p-tol)4C4SnMe2 in deoxygenated CCl4 treated with PhBCl2, whole exchange complete in 15 min; not isolated; detected by NMR;
DOI:10.1021/ja00263a006

Reference yield:

: 2789-88-0
1,2-bis(4-methylphenyl)acetylene

: 99643-61-5
1-phenyl-2,3,4,5-tetra-p-tolylborole

Guidance literature:: Multi-step reaction with 2 steps

1: lithium / diethyl ether; tetrahydrofuran

2: toluene

With lithium; In tetrahydrofuran; diethyl ether; toluene;
DOI:10.1021/ja00263a006