N-(7-{[3-O-(aminocarbonyl)-6-deoxy-2-O-acetyl-5-C-methyl-4-O-methyl-α-L-lyxo-hexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxybenzamide

Base Information

Chemical Name:N-(7-{[3-O-(aminocarbonyl)-6-deoxy-2-O-acetyl-5-C-methyl-4-O-methyl-α-L-lyxo-hexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxybenzamide
CAS No.:1449759-53-8
Molecular Formula:C₂₈H₃₀N₂O₁₂
Molecular Weight:586.552
Hs Code.:

N-(7-{[3-O-(aminocarbonyl)-6-deoxy-2-O-acetyl-5-C-methyl-4-O-methyl-α-L-lyxo-hexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxybenzamide

Synonyms:N-(7-{[3-O-(aminocarbonyl)-6-deoxy-2-O-acetyl-5-C-methyl-4-O-methyl-α-L-lyxo-hexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxybenzamide

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Chemical Property of N-(7-{[3-O-(aminocarbonyl)-6-deoxy-2-O-acetyl-5-C-methyl-4-O-methyl-α-L-lyxo-hexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxybenzamide

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Technology Process of N-(7-{[3-O-(aminocarbonyl)-6-deoxy-2-O-acetyl-5-C-methyl-4-O-methyl-α-L-lyxo-hexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxybenzamide

There total 5 articles about N-(7-{[3-O-(aminocarbonyl)-6-deoxy-2-O-acetyl-5-C-methyl-4-O-methyl-α-L-lyxo-hexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1449759-52-7
C₃₅H₃₆N₂O₁₂

: 1449759-53-8
N-(7-{[3-O-(aminocarbonyl)-6-deoxy-2-O-acetyl-5-C-methyl-4-O-methyl-α-L-lyxo-hexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxybenzamide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 4h;
DOI:10.1016/j.bmc.2013.06.042

Reference yield:

: 116635-17-7
1-<(2,6-dimethyl-4-oxo-4H-<1>benzopyrano<3,4-d>oxazol-7-yl)oxy>-2-acetoxy-4-methoxy-5,5-dimethyl-3-tetrahydropyranyl 5-methyl-1H-pyrrole-2-carboxylate

: 1449759-53-8
N-(7-{[3-O-(aminocarbonyl)-6-deoxy-2-O-acetyl-5-C-methyl-4-O-methyl-α-L-lyxo-hexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / 3 h / Reflux

2.1: dicyclohexyl-carbodiimide; 4-pyrrolidin-1-ylpyridine / ethanol / 0.5 h / 25 °C

2.2: 25 °C

3.1: palladium 10% on activated carbon; hydrogen / ethanol / 4 h / 20 °C

With palladium 10% on activated carbon; hydrogen; 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In ethanol;
DOI:10.1016/j.bmc.2013.06.042

Reference yield:

: 1476-53-5,6990-02-9,18656-99-0
sodium novobiocin

: 1449759-53-8
N-(7-{[3-O-(aminocarbonyl)-6-deoxy-2-O-acetyl-5-C-methyl-4-O-methyl-α-L-lyxo-hexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxybenzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride / water

2.1: pyridine / 24 h / Reflux

3.1: ethanol / 3 h / Reflux

4.1: dicyclohexyl-carbodiimide; 4-pyrrolidin-1-ylpyridine / ethanol / 0.5 h / 25 °C

4.2: 25 °C

5.1: palladium 10% on activated carbon; hydrogen / ethanol / 4 h / 20 °C

With pyridine; hydrogenchloride; palladium 10% on activated carbon; hydrogen; 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In ethanol; water;
DOI:10.1016/j.bmc.2013.06.042