N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxy benzamide

Base Information

Chemical Name:N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxy benzamide
CAS No.:56786-00-6
Molecular Formula:C₂₆H₂₈N₂O₁₁
Molecular Weight:544.515
Hs Code.:

N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxy benzamide

Synonyms:N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxy benzamide

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Chemical Property of N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxy benzamide

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Technology Process of N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxy benzamide

There total 6 articles about N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxy benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1449759-53-8
N-(7-{[3-O-(aminocarbonyl)-6-deoxy-2-O-acetyl-5-C-methyl-4-O-methyl-α-L-lyxo-hexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxybenzamide

: 56786-00-6
N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxy benzamide

Guidance literature:: With sodium cyanide; In methanol; at 25 ℃;
DOI:10.1016/j.bmc.2013.06.042

Reference yield:

: 116635-17-7
1-<(2,6-dimethyl-4-oxo-4H-<1>benzopyrano<3,4-d>oxazol-7-yl)oxy>-2-acetoxy-4-methoxy-5,5-dimethyl-3-tetrahydropyranyl 5-methyl-1H-pyrrole-2-carboxylate

: 56786-00-6
N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxy benzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: ethanol / 3 h / Reflux

2.1: dicyclohexyl-carbodiimide; 4-pyrrolidin-1-ylpyridine / ethanol / 0.5 h / 25 °C

2.2: 25 °C

3.1: palladium 10% on activated carbon; hydrogen / ethanol / 4 h / 20 °C

4.1: sodium cyanide / methanol / 25 °C

With sodium cyanide; palladium 10% on activated carbon; hydrogen; 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In methanol; ethanol;
DOI:10.1016/j.bmc.2013.06.042

Reference yield:

: 7-{[2-O-acetyl-3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-l-lyxo-hexopyranosyl]oxy}-3-amino-4-hydroxy-8-methyl-2H-1-benzopyran-2-one

: 56786-00-6
N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-hydroxy benzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: dicyclohexyl-carbodiimide; 4-pyrrolidin-1-ylpyridine / ethanol / 0.5 h / 25 °C

1.2: 25 °C

2.1: palladium 10% on activated carbon; hydrogen / ethanol / 4 h / 20 °C

3.1: sodium cyanide / methanol / 25 °C

With sodium cyanide; palladium 10% on activated carbon; hydrogen; 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In methanol; ethanol;
DOI:10.1016/j.bmc.2013.06.042