2-carboxy-5,7-dichloro-4-[4-(N,N-dimethylaminomethyl)benzylcarbonylamino]-1,2,3,4-tetrahydroquinoline

Base Information

Chemical Name:2-carboxy-5,7-dichloro-4-[4-(N,N-dimethylaminomethyl)benzylcarbonylamino]-1,2,3,4-tetrahydroquinoline
CAS No.:132689-35-1
Molecular Formula:C₂₁H₂₃Cl₂N₃O₃
Molecular Weight:436.338
Hs Code.:

Synonyms:2-carboxy-5,7-dichloro-4-[4-(N,N-dimethylaminomethyl)benzylcarbonylamino]-1,2,3,4-tetrahydroquinoline

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Chemical Property of 2-carboxy-5,7-dichloro-4-[4-(N,N-dimethylaminomethyl)benzylcarbonylamino]-1,2,3,4-tetrahydroquinoline

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 2-carboxy-5,7-dichloro-4-[4-(N,N-dimethylaminomethyl)benzylcarbonylamino]-1,2,3,4-tetrahydroquinoline

There total 4 articles about 2-carboxy-5,7-dichloro-4-[4-(N,N-dimethylaminomethyl)benzylcarbonylamino]-1,2,3,4-tetrahydroquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

aqueous lithium hydroxide: aqueous lithium hydroxide

: 132689-34-0
5,7-dichloro-4-[4-(N,N-dimethylaminomethyl)benzylcarbonylamino]-2-methoxycarbonyl-1,2,3,4-tetrahydroquinoline

: 132689-35-1
2-carboxy-5,7-dichloro-4-[4-(N,N-dimethylaminomethyl)benzylcarbonylamino]-1,2,3,4-tetrahydroquinoline

Guidance literature:: In tetrahydrofuran; water;

Reference yield:

: 132691-22-6
ethyl 4-(N,N-dimethylaminomethyl)phenylacetate

: 132689-35-1
2-carboxy-5,7-dichloro-4-[4-(N,N-dimethylaminomethyl)benzylcarbonylamino]-1,2,3,4-tetrahydroquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran; water

2: benzotriazol-1-ol / tetrahydrofuran; dichloromethane; water; ethyl acetate

3: tetrahydrofuran; water

With benzotriazol-1-ol; In tetrahydrofuran; dichloromethane; water; ethyl acetate;

Reference yield:

: 17841-69-9
ethyl 4-(aminomethyl)phenylacetate hydrochloride

: 132689-35-1
2-carboxy-5,7-dichloro-4-[4-(N,N-dimethylaminomethyl)benzylcarbonylamino]-1,2,3,4-tetrahydroquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: formaldehyd; sodium cyanoborohydride; sodium carbonate / water; acetonitrile

2: tetrahydrofuran; water

3: benzotriazol-1-ol / tetrahydrofuran; dichloromethane; water; ethyl acetate

4: tetrahydrofuran; water

With formaldehyd; sodium cyanoborohydride; sodium carbonate; benzotriazol-1-ol; In tetrahydrofuran; dichloromethane; water; ethyl acetate; acetonitrile;