(5-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanol

Base Information

• Chemical Name: (5-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanol
• CAS No.: 249762-29-6
• Molecular Formula: C₃₀H₂₄N₂O₆S₂
• Molecular Weight: 572.662

Synonyms:(5-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanol

Chemical Property of (5-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanol

Chemical Property:

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Technology Process of (5-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanol

There total 1 articles about (5-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

1-benzenesulfonyl-5-methoxy-1H-indole (56995-12-1) + 1-(phenylsulfonyl)-1H-indole-2-carbaldehyde (80360-23-2) → (5-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanol (249762-29-6)

Guidance literature:

1-benzenesulfonyl-5-methoxy-1H-indole; With n-butyllithium; diisopropylamine; In tetrahydrofuran; at 0 ℃; for 0.5h;

1-(phenylsulfonyl)-1H-indole-2-carbaldehyde; In tetrahydrofuran; at -78 - 20 ℃; Further stages.;

DOI:10.1021/jm010988n

Reference yield: 63.0%

(5-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanol (249762-29-6) → (5-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanone (249762-40-1)

Guidance literature:

With dipyridinium dichromate; pyridinium trifluroacetate; In dichloromethane; at 20 ℃;

DOI:10.1021/jm010988n

Reference yield: 56.0%

(5-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanol (249762-29-6) → (5-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methane

Guidance literature:

With trifluoroacetic acid; HSiPh₃; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/jo981926g

upstream raw materials:

1-benzenesulfonyl-5-methoxy-1H-indole

1-(phenylsulfonyl)-1H-indole-2-carbaldehyde

Downstream raw materials:

(5-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanone

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