1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-6-O-methyl-3-O-<(trifluormethyl)sulfonyl>-myo-inosit

Base Information

Chemical Name:1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-6-O-methyl-3-O-<(trifluormethyl)sulfonyl>-myo-inosit
CAS No.:97119-72-7
Molecular Formula:C₃₇H₃₉F₃O₈S
Molecular Weight:708.71
Hs Code.:

1L-2,4,5,7-Tetra-O-<D2>benzyl-1-desoxy-1-C-(hydroxymethyl)-6-O-methyl-3-O-<(trifluormethyl)sulfonyl>-myo-inosit

Synonyms:1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-6-O-methyl-3-O-<(trifluormethyl)sulfonyl>-myo-inosit

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Chemical Property of 1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-6-O-methyl-3-O-<(trifluormethyl)sulfonyl>-myo-inosit

Chemical Property:

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Technology Process of 1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-6-O-methyl-3-O-<(trifluormethyl)sulfonyl>-myo-inosit

There total 14 articles about 1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-6-O-methyl-3-O-<(trifluormethyl)sulfonyl>-myo-inosit which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 97119-71-6
1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-6-O-methyl-myo-inosit

: 97119-72-7
1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-6-O-methyl-3-O-<(trifluormethyl)sulfonyl>-myo-inosit

Guidance literature:: With pyridine; In dichloromethane; at -40 ℃;

Reference yield:

: 51271-29-5
[1',1'-2H₂]benzyl bromide

: 97119-72-7
1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-6-O-methyl-3-O-<(trifluormethyl)sulfonyl>-myo-inosit

Guidance literature:: Multi-step reaction with 11 steps

1: 94 percent / 1) NaH / dimethylformamide / 1) 2 h, 0 deg C, 2) 5 h, room temp.

2: 81 percent / 98percent acetic acid / 30 °C

3: 91 percent / 1) NaH / dimethylformamide / 1) 2 h, 0 deg C, 2) 5 h, room temp.

4: 91 percent / acetic acid / tetrahydrofuran; H₂O / 60 °C

5: p-toluenesulfonic acid / toluene / 0.17 h / Ambient temperature

6: 90percent acetic acid / toluene / 0.08 h

7: 89 percent / ethyldiisopropylamine / CH₂Cl₂

8: 1 N NaOCH₃ / methanol

9: 91 percent / 1) NaH / dimethylformamide / 1) 2 h, 0 deg C, 2) 5 h, room temp.

10: 95 percent / 3 N HCl / tetrahydrofuran / 10 h / 60 °C

11: 89 percent / pyridine / CH₂Cl₂ / -40 °C

With pyridine; hydrogenchloride; sodium methylate; sodium hydride; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 86845-47-8,86853-27-2
1L-1-Desoxy-1-C-hydroxymethyl-2,3:4,5-di-O-isopropyliden-6-O-methyl-myo-inosit

: 97119-72-7
1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-6-O-methyl-3-O-<(trifluormethyl)sulfonyl>-myo-inosit

Guidance literature:: Multi-step reaction with 11 steps

1: 94 percent / 1) NaH / dimethylformamide / 1) 2 h, 0 deg C, 2) 5 h, room temp.

2: 81 percent / 98percent acetic acid / 30 °C

3: 91 percent / 1) NaH / dimethylformamide / 1) 2 h, 0 deg C, 2) 5 h, room temp.

4: 91 percent / acetic acid / tetrahydrofuran; H₂O / 60 °C

5: p-toluenesulfonic acid / toluene / 0.17 h / Ambient temperature

6: 90percent acetic acid / toluene / 0.08 h

7: 89 percent / ethyldiisopropylamine / CH₂Cl₂

8: 1 N NaOCH₃ / methanol

9: 91 percent / 1) NaH / dimethylformamide / 1) 2 h, 0 deg C, 2) 5 h, room temp.

10: 95 percent / 3 N HCl / tetrahydrofuran / 10 h / 60 °C

11: 89 percent / pyridine / CH₂Cl₂ / -40 °C

With pyridine; hydrogenchloride; sodium methylate; sodium hydride; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;