Th₂CONHPh

Base Information

• Chemical Name: Th₂CONHPh
• CAS No.: 1258875-44-3
• Molecular Formula: C₂₀H₂₁NOS₂
• Molecular Weight: 355.525

Synonyms:Th₂CONHPh

Chemical Property of Th₂CONHPh

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of Th₂CONHPh

There total 1 articles about Th₂CONHPh which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

aniline (62-53-3) + 2-chloro-1,2-bis[2,5-dimethyl(3-thienyl)]ethan-1-one (252264-76-9) → Th2CONHPh (1258875-44-3)

Guidance literature:

With potassium carbonate; sodium iodide; In acetonitrile; at 60 - 70 ℃; Inert atmosphere;

DOI:10.1002/chem.201001319

Reference yield: 80.0%

Th2CONHPh (1258875-44-3) + acetyl chloride (75-36-5) → C22H23NO2S2 (1258875-46-5)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1002/chem.201001319

Reference yield: 66.0%

Th2CONHPh (1258875-44-3) + ethyl trifluoroacetaldehyde hemiacetal (433-27-2) → C22H19F3N2S2 (1258875-65-8)

Guidance literature:

With ammonium acetate; In acetic acid; for 20h; Reflux;

DOI:10.1002/chem.201001319

upstream raw materials:

aniline

2-chloro-1,2-bis[2,5-dimethyl(3-thienyl)]ethan-1-one

Downstream raw materials:

C₂₁H₂₁NO₂S₂

C₂₂H₂₃NO₂S₂

C₂₂H₁₉F₃N₂S₂

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