tert-Butoxycarbonylamino-acetic acid 4-(benzyloxycarbonylamino-imino-methyl)-phenyl ester

Base Information

Chemical Name:tert-Butoxycarbonylamino-acetic acid 4-(benzyloxycarbonylamino-imino-methyl)-phenyl ester
CAS No.:76224-01-6
Molecular Formula:C₂₂H₂₅N₃O₆
Molecular Weight:427.457
Hs Code.:

Synonyms:tert-Butoxycarbonylamino-acetic acid 4-(benzyloxycarbonylamino-imino-methyl)-phenyl ester

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Chemical Property of tert-Butoxycarbonylamino-acetic acid 4-(benzyloxycarbonylamino-imino-methyl)-phenyl ester

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Technology Process of tert-Butoxycarbonylamino-acetic acid 4-(benzyloxycarbonylamino-imino-methyl)-phenyl ester

There total 3 articles about tert-Butoxycarbonylamino-acetic acid 4-(benzyloxycarbonylamino-imino-methyl)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 4530-20-5
BOC-glycine

: 76223-53-5
N-(benzyloxycarbonyl)-p-amidinophenol

: 76224-01-6
tert-Butoxycarbonylamino-acetic acid 4-(benzyloxycarbonylamino-imino-methyl)-phenyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; acetonitrile; Ambient temperature;

Reference yield:

: 38148-63-9
p-amidinophenol hydrochloride

: 76224-01-6
tert-Butoxycarbonylamino-acetic acid 4-(benzyloxycarbonylamino-imino-methyl)-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / Et₃N / dimethylformamide / 2 h / Ambient temperature

2: 81 percent / 5percent NaOH / ethanol / 1.5 h / Ambient temperature

3: 85 percent / DCC, 4-dimethylaminopyridine / acetonitrile; dimethylformamide / Ambient temperature

With dmap; sodium hydroxide; triethylamine; dicyclohexyl-carbodiimide; In ethanol; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 76223-55-7
N,O-bis(benzyloxycarbonyl)-p-amidinophenol

: 76224-01-6
tert-Butoxycarbonylamino-acetic acid 4-(benzyloxycarbonylamino-imino-methyl)-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / 5percent NaOH / ethanol / 1.5 h / Ambient temperature

2: 85 percent / DCC, 4-dimethylaminopyridine / acetonitrile; dimethylformamide / Ambient temperature

With dmap; sodium hydroxide; dicyclohexyl-carbodiimide; In ethanol; N,N-dimethyl-formamide; acetonitrile;