Allyl-[(Z)-2-((R)-toluene-4-sulfinyl)-1-trifluoromethyl-vinyl]-carbamic acid benzyl ester

Base Information

Chemical Name:Allyl-[(Z)-2-((R)-toluene-4-sulfinyl)-1-trifluoromethyl-vinyl]-carbamic acid benzyl ester
CAS No.:177267-98-0
Molecular Formula:C₂₁H₂₀F₃NO₃S
Molecular Weight:423.456
Hs Code.:

Synonyms:Allyl-[(Z)-2-((R)-toluene-4-sulfinyl)-1-trifluoromethyl-vinyl]-carbamic acid benzyl ester

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Chemical Property of Allyl-[(Z)-2-((R)-toluene-4-sulfinyl)-1-trifluoromethyl-vinyl]-carbamic acid benzyl ester

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Technology Process of Allyl-[(Z)-2-((R)-toluene-4-sulfinyl)-1-trifluoromethyl-vinyl]-carbamic acid benzyl ester

There total 7 articles about Allyl-[(Z)-2-((R)-toluene-4-sulfinyl)-1-trifluoromethyl-vinyl]-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 106-95-6
allyl bromide

: 169137-91-1
[(Z)-2-((R)-Toluene-4-sulfinyl)-1-trifluoromethyl-vinyl]-carbamic acid benzyl ester

: 177267-98-0
Allyl-[(Z)-2-((R)-toluene-4-sulfinyl)-1-trifluoromethyl-vinyl]-carbamic acid benzyl ester

Guidance literature:: With potassium carbonate; In 1,4-dioxane; water; for 48h; Ambient temperature;
DOI:10.1021/jo952097r

Reference yield:

: 113965-64-3
1,1,1-Trifluoro-3-((R)-toluene-4-sulfinyl)-propan-2-one

: 177267-98-0
Allyl-[(Z)-2-((R)-toluene-4-sulfinyl)-1-trifluoromethyl-vinyl]-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: toluene; benzene / Ambient temperature

2: 1.) n-butyllithium / 1.) THF, hexane, -78 deg C, 15 min, 2.) THF, hexane, -78 deg C, 5 min

3: 76 percent / K₂CO₃ / dioxane; H₂O / 48 h / Ambient temperature

With n-butyllithium; potassium carbonate; In 1,4-dioxane; water; toluene; benzene;
DOI:10.1021/jo952097r

Reference yield:

: 81357-08-6
benzyl (triphenyl-λ⁵-phosphanilidene)carbamate

: 177267-98-0
Allyl-[(Z)-2-((R)-toluene-4-sulfinyl)-1-trifluoromethyl-vinyl]-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / benzene / 20 h / Heating

2: 76 percent / K₂CO₃ / dioxane; H₂O / 48 h / Ambient temperature

With potassium carbonate; In 1,4-dioxane; water; benzene;
DOI:10.1021/jo952097r