{((C₆H₅)3P)2N}⁽¹⁺⁾*{HFe₃(CO)9BH₃}^(1-)={((C₆H₅)3P)2N}{HFe₃(CO)9BH₃}

Base Information

Chemical Name:{((C₆H₅)3P)2N}⁽¹⁺⁾*{HFe₃(CO)9BH₃}^(1-)={((C₆H₅)3P)2N}{HFe₃(CO)9BH₃}
CAS No.:92055-46-4
Molecular Formula:C₉H₄BFe₃O₉*C₃₆H₃₀NP₂
Molecular Weight:973.066
Hs Code.:

{((C<sub>6</sub>H<sub>5</sub>)3P)2N}<sup>(1+)</sup>*{HFe<sub>3</sub>(CO)9BH<sub>3</sub>}<sup>(1-)</sup>={((C<sub>6</sub>H<sub>5</sub>)3P)2N}{HFe<sub>3</sub>(CO)9BH<sub>3</sub>}

Synonyms:{((C₆H₅)3P)2N}⁽¹⁺⁾*{HFe₃(CO)9BH₃}^(1-)={((C₆H₅)3P)2N}{HFe₃(CO)9BH₃}

Suppliers and Price of {((C₆H₅)3P)2N}⁽¹⁺⁾*{HFe₃(CO)9BH₃}^(1-)={((C₆H₅)3P)2N}{HFe₃(CO)9BH₃}

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of {((C₆H₅)3P)2N}⁽¹⁺⁾*{HFe₃(CO)9BH₃}^(1-)={((C₆H₅)3P)2N}{HFe₃(CO)9BH₃}

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of {((C₆H₅)3P)2N}⁽¹⁺⁾*{HFe₃(CO)9BH₃}^(1-)={((C₆H₅)3P)2N}{HFe₃(CO)9BH₃}

There total 1 articles about {((C₆H₅)3P)2N}⁽¹⁺⁾*{HFe₃(CO)9BH₃}^(1-)={((C₆H₅)3P)2N}{HFe₃(CO)9BH₃} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: {bis(triphenylphosphine)iminium}{Me(carbonyl)iron(carbonyl)4}

: borane tetrahydrofuran

: 92055-46-4
{((C₆H₅)3P)2N}⁽¹⁺⁾*{HFe₃(CO)9BH₃}^(1-)={((C₆H₅)3P)2N}{HFe₃(CO)9BH₃}

Guidance literature:: With H₃PO₄; In hexane; during 1 min BF3*THF (6 mmol) was added to a suspn. of ((CO)4FeC(O)CH3)(((C6H5)3P)2N) (2 mmol) in hexane at 25°C under N2; the mixt. washeld at 60°C for 2 h with stirring, then it was cooled to room temp.; acidification with aq. H3PO4; removing of the hexane from soln., extn. with toluene, sepn. by chromy.(CH2Cl2:toluene (4:1) eluent);
DOI:10.1021/ja00272a026

Reference yield: 80.0%

: 92055-46-4
{((C₆H₅)3P)2N}⁽¹⁺⁾*{HFe₃(CO)9BH₃}^(1-)={((C₆H₅)3P)2N}{HFe₃(CO)9BH₃}

: 102233-78-3
(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*(Fe₃(CO)9(CO)BH₂)^(1-)=((C₆H₅)3PNP(C₆H₅)3)(Fe₃(CO)9(CO)BH₂)

Guidance literature:: With carbon monoxide; In toluene; CO bubbled through soln. PPN(Fe3(CO)9(H)BH3) in toluene at 45°C for 40 h;
DOI:10.1021/ja00276a026

Reference yield: 67.0%

: 92055-46-4
{((C₆H₅)3P)2N}⁽¹⁺⁾*{HFe₃(CO)9BH₃}^(1-)={((C₆H₅)3P)2N}{HFe₃(CO)9BH₃}

: 672-66-2
Dimethyl(phenyl)phosphine

: 102233-80-7
(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*Fe₃BH₂^(1-)*9CO*((C₆H₅)(CH₃)2P)=((C₆H₅)3PNP(C₆H₅)3)(Fe₃(CO)8(CO)((C₆H₅)(CH₃)2P)BH₂)

Guidance literature:: In acetone; soln. PhMe2P in acetone added to soln. (Fe3(CO)9(H)BH3)(PPN) in acetoneat room temp. and mixt. allowed to react for 30 h;
DOI:10.1021/ja00276a026