N-[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-N'-(3-bromo-5-tert-butyl-2-methoxyphenyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine

Base Information

• Chemical Name: N-[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-N'-(3-bromo-5-tert-butyl-2-methoxyphenyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine
• CAS No.: 1041862-65-0
• Molecular Formula: C₄₄H₅₉Br₂N₃O₄
• Molecular Weight: 853.778
• Mol file: 1041862-65-0.mol

Synonyms:N-[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-N'-(3-bromo-5-tert-butyl-2-methoxyphenyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine

Chemical Property of N-[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-N'-(3-bromo-5-tert-butyl-2-methoxyphenyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-N'-(3-bromo-5-tert-butyl-2-methoxyphenyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine

There total 1 articles about N-[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-N'-(3-bromo-5-tert-butyl-2-methoxyphenyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

N,N'-bis(3-bromo-5-tert-butyl-2-methoxyphenyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine (854669-22-0) + 3-bromo-5-(tert-butyl)-2-methoxyaniline (1041054-73-2) → N-[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-N'-(3-bromo-5-tert-butyl-2-methoxyphenyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine (1041862-65-0)

Guidance literature:

With palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate; In toluene; at 80 ℃; for 15h; Inert atmosphere;

DOI:10.1039/b801127c

Reference yield: 88.0%

N-[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-N'-(3-bromo-5-tert-butyl-2-methoxyphenyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine (1041862-65-0) + methyl iodide (74-88-4) → N-[3-(3-bromo-5-tert-butyl-2-methoxy-N''-methylanilino)-5-tert-butyl-2-methoxyphenyl]-N'-(3-bromo-5-tert-butyl-2-methoxyphenyl)-5-tert-butyl-2-methoxy-N,N'-dimethyl-1,3-phenylenediamine (1041862-62-7)

Guidance literature:

N-[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-N'-(3-bromo-5-tert-butyl-2-methoxyphenyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.166667h; Inert atmosphere;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; Inert atmosphere;

DOI:10.1039/b801127c

upstream raw materials:

N,N'-bis(3-bromo-5-tert-butyl-2-methoxyphenyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine

3-bromo-5-(tert-butyl)-2-methoxyaniline

Downstream raw materials:

N-[3-(3-bromo-5-tert-butyl-2-methoxy-N''-methylanilino)-5-tert-butyl-2-methoxyphenyl]-N'-(3-bromo-5-tert-butyl-2-methoxyphenyl)-5-tert-butyl-2-methoxy-N,N'-dimethyl-1,3-phenylenediamine