[(5-[1,3]dioxolan-2-yl-2,3,4-trimethoxyphenyl)-(4-phenoxyphenyl)]methanol

Base Information

• Chemical Name: [(5-[1,3]dioxolan-2-yl-2,3,4-trimethoxyphenyl)-(4-phenoxyphenyl)]methanol
• CAS No.: 1011708-98-7
• Molecular Formula: C₂₅H₂₆O₇
• Molecular Weight: 438.477

Synonyms:[(5-[1,3]dioxolan-2-yl-2,3,4-trimethoxyphenyl)-(4-phenoxyphenyl)]methanol

Chemical Property of [(5-[1,3]dioxolan-2-yl-2,3,4-trimethoxyphenyl)-(4-phenoxyphenyl)]methanol

Chemical Property:

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Technology Process of [(5-[1,3]dioxolan-2-yl-2,3,4-trimethoxyphenyl)-(4-phenoxyphenyl)]methanol

There total 2 articles about [(5-[1,3]dioxolan-2-yl-2,3,4-trimethoxyphenyl)-(4-phenoxyphenyl)]methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

5-([1,3]dioxolan-2-yl)-2,3,4-trimethoxybenzaldehyde (1011708-97-6) + 4-phenoxyphenylmagnesium bromide (21473-02-9) → [(5-[1,3]dioxolan-2-yl-2,3,4-trimethoxyphenyl)-(4-phenoxyphenyl)]methanol (1011708-98-7)

Guidance literature:

In tetrahydrofuran; at 0 - 20 ℃; for 3h;

DOI:10.1021/jm701358v

Reference yield:

5-([1,3]dioxolan-2-yl)-2,3,4-trimethoxybenzaldehyde (1011708-97-6) → [(5-[1,3]dioxolan-2-yl-2,3,4-trimethoxyphenyl)-(4-phenoxyphenyl)]methanol (1011708-98-7)

Guidance literature:

Reference yield: 86.0%

[(5-[1,3]dioxolan-2-yl-2,3,4-trimethoxyphenyl)-(4-phenoxyphenyl)]methanol (1011708-98-7) → 5-[hydroxy-(4-phenoxyphenyl)methyl]-2,3,4-trimethoxybenzaldehyde (1011708-99-8)

Guidance literature:

With toluene-4-sulfonic acid; In acetone; at 0 ℃; for 0.333333h;

DOI:10.1021/jm701358v

upstream raw materials:

5-([1,3]dioxolan-2-yl)-2,3,4-trimethoxybenzaldehyde

4-phenoxyphenylmagnesium bromide

Downstream raw materials:

5-[hydroxy-(4-phenoxyphenyl)methyl]-2,3,4-trimethoxybenzaldehyde

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