N-tert-butyloxycarbonyl-N-(2-methylene cyclohexyl)benzenesulfenamide

Base Information

Chemical Name:N-tert-butyloxycarbonyl-N-(2-methylene cyclohexyl)benzenesulfenamide
CAS No.:267668-28-0
Molecular Formula:C₁₈H₂₅NO₂S
Molecular Weight:319.468
Hs Code.:

Synonyms:N-tert-butyloxycarbonyl-N-(2-methylene cyclohexyl)benzenesulfenamide

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Chemical Property of N-tert-butyloxycarbonyl-N-(2-methylene cyclohexyl)benzenesulfenamide

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Technology Process of N-tert-butyloxycarbonyl-N-(2-methylene cyclohexyl)benzenesulfenamide

There total 4 articles about N-tert-butyloxycarbonyl-N-(2-methylene cyclohexyl)benzenesulfenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1070-19-5
N-(tert-butyloxycarbonyl) azide

: 79597-48-1
1-cyclohexenylmethyl phenyl sulfide

: 267668-28-0
N-tert-butyloxycarbonyl-N-(2-methylene cyclohexyl)benzenesulfenamide

Guidance literature:: With iron(II) chloride; In dichloromethane; at 20 ℃;
DOI:10.1021/jo991569p

Reference yield:

: 100-68-5
methyl-phenyl-thioether

: 267668-28-0
N-tert-butyloxycarbonyl-N-(2-methylene cyclohexyl)benzenesulfenamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi / hexane; tetrahydrofuran / 0 - 20 °C

1.2: tetrahydrofuran / 2.5 h / 20 °C

2.1: 3.1 g / p-toluenesulfonic acid / benzene / 4 h / Heating

3.1: 65 percent / FeCl₂ / CH₂Cl₂ / 20 °C

With n-butyllithium; toluene-4-sulfonic acid; iron(II) chloride; In tetrahydrofuran; hexane; dichloromethane; benzene; 1.1: Metallation / 1.2: Addition / 2.1: Elimination / 3.1: Rearrangement;
DOI:10.1021/jo991569p

Reference yield:

: 101704-19-2
1-((phenylthio)methyl)cyclohexanol

: 267668-28-0
N-tert-butyloxycarbonyl-N-(2-methylene cyclohexyl)benzenesulfenamide

Guidance literature:: Multi-step reaction with 2 steps

1: 3.1 g / p-toluenesulfonic acid / benzene / 4 h / Heating

2: 65 percent / FeCl₂ / CH₂Cl₂ / 20 °C

With toluene-4-sulfonic acid; iron(II) chloride; In dichloromethane; benzene; 1: Elimination / 2: Rearrangement;
DOI:10.1021/jo991569p