Oxo-phenyl-acetic acid (S)-1-benzyl-4-methyl-1,4-dihydro-pyridin-3-ylmethyl ester

Base Information

Chemical Name:Oxo-phenyl-acetic acid (S)-1-benzyl-4-methyl-1,4-dihydro-pyridin-3-ylmethyl ester
CAS No.:108214-23-9
Molecular Formula:C₂₂H₂₁NO₃
Molecular Weight:347.414
Hs Code.:

Synonyms:Oxo-phenyl-acetic acid (S)-1-benzyl-4-methyl-1,4-dihydro-pyridin-3-ylmethyl ester

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Chemical Property of Oxo-phenyl-acetic acid (S)-1-benzyl-4-methyl-1,4-dihydro-pyridin-3-ylmethyl ester

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Technology Process of Oxo-phenyl-acetic acid (S)-1-benzyl-4-methyl-1,4-dihydro-pyridin-3-ylmethyl ester

There total 1 articles about Oxo-phenyl-acetic acid (S)-1-benzyl-4-methyl-1,4-dihydro-pyridin-3-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25726-04-9
phenylglyoxylyl chloride

: 101031-31-6
S-(+)-1-benzyl-3-hydroxymethyl-4-methyl-1,4-dihydropyridine

: 108214-23-9
Oxo-phenyl-acetic acid (S)-1-benzyl-4-methyl-1,4-dihydro-pyridin-3-ylmethyl ester

Guidance literature:: With potassium hydride; In tetrahydrofuran;
DOI:10.1021/ja00244a054

Reference yield:

: 108214-23-9
Oxo-phenyl-acetic acid (S)-1-benzyl-4-methyl-1,4-dihydro-pyridin-3-ylmethyl ester

: 21210-43-5
(S)-Methyl mandelate

Guidance literature:: Multi-step reaction with 2 steps

1: Mg(ClO₄)2 / 96 h

2: 65 percent / methanol

With magnesium(II) perchlorate; In methanol;
DOI:10.1021/ja00244a054

Reference yield:

: 108214-23-9
Oxo-phenyl-acetic acid (S)-1-benzyl-4-methyl-1,4-dihydro-pyridin-3-ylmethyl ester

: 20698-91-3
(R)-methyl mandelate

Guidance literature:: Multi-step reaction with 2 steps

1: Mg(ClO₄)2 / 96 h

2: methanol

With magnesium(II) perchlorate; In methanol;
DOI:10.1021/ja00244a054