4-methanesulfonyl-7-(4-methanesulfonylphenyl)thieno[3,2-d]pyrimidine

Base Information

Chemical Name:4-methanesulfonyl-7-(4-methanesulfonylphenyl)thieno[3,2-d]pyrimidine
CAS No.:1384951-70-5
Molecular Formula:C₁₄H₁₂N₂O₄S₃
Molecular Weight:368.458
Hs Code.:

Synonyms:4-methanesulfonyl-7-(4-methanesulfonylphenyl)thieno[3,2-d]pyrimidine

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Chemical Property of 4-methanesulfonyl-7-(4-methanesulfonylphenyl)thieno[3,2-d]pyrimidine

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Technology Process of 4-methanesulfonyl-7-(4-methanesulfonylphenyl)thieno[3,2-d]pyrimidine

There total 5 articles about 4-methanesulfonyl-7-(4-methanesulfonylphenyl)thieno[3,2-d]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1384951-69-2
7-(4-methanesulfonylphenyl)-4-methylsulfanylthieno[3,2-d]pyrimidine

: 1384951-70-5
4-methanesulfonyl-7-(4-methanesulfonylphenyl)thieno[3,2-d]pyrimidine

Guidance literature:: 7-(4-methanesulfonylphenyl)-4-methylsulfanylthieno[3,2-d]pyrimidine; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 1h;

With sodium hydrogencarbonate; In dichloromethane; at 20 ℃;

Reference yield:

: 31169-27-4
7-bromo-4-chlorothieno[3,2-d]pyrimidine

: 1384951-70-5
4-methanesulfonyl-7-(4-methanesulfonylphenyl)thieno[3,2-d]pyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 13 h / 10 - 20 °C

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 4 h / 100 °C / Inert atmosphere

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 0 °C

3.2: 20 °C

With sodium carbonate; 3-chloro-benzenecarboperoxoic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;

Reference yield:

: 16234-10-9
3H-thieno[3,2-d]pyrimidin-4-one

: 1384951-70-5
4-methanesulfonyl-7-(4-methanesulfonylphenyl)thieno[3,2-d]pyrimidine

Guidance literature:: Multi-step reaction with 5 steps

1.1: bromine / acetic acid / 12 h / 120 °C / Sealed reactor

2.1: trichlorophosphate / 3 h / 150 °C

3.1: tetrahydrofuran / 13 h / 10 - 20 °C

4.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 4 h / 100 °C / Inert atmosphere

5.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 0 °C

5.2: 20 °C

With bromine; sodium carbonate; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; acetic acid;