O²-(2,4-dinitro-5-fluorophenyl) 1-(4-methylpiperazin-1-yl)diazen-1-ium-1,2-diolate

Base Information

• Chemical Name: O²-(2,4-dinitro-5-fluorophenyl) 1-(4-methylpiperazin-1-yl)diazen-1-ium-1,2-diolate
• CAS No.: 1434556-64-5
• Molecular Formula: C₁₁H₁₃FN₆O₆
• Molecular Weight: 344.259

Synonyms:O²-(2,4-dinitro-5-fluorophenyl) 1-(4-methylpiperazin-1-yl)diazen-1-ium-1,2-diolate

Chemical Property of O²-(2,4-dinitro-5-fluorophenyl) 1-(4-methylpiperazin-1-yl)diazen-1-ium-1,2-diolate

Chemical Property:

Purity/Quality:

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Technology Process of O²-(2,4-dinitro-5-fluorophenyl) 1-(4-methylpiperazin-1-yl)diazen-1-ium-1,2-diolate

There total 2 articles about O²-(2,4-dinitro-5-fluorophenyl) 1-(4-methylpiperazin-1-yl)diazen-1-ium-1,2-diolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

sodium 1-(4-methylpiperazin-1-yl)diazen-1-ium-1,2-diolate + 1,5-difluoro-2,4-dinitrobenzene (327-92-4) → O2-(2,4-dinitro-5-fluorophenyl) 1-(4-methylpiperazin-1-yl)diazen-1-ium-1,2-diolate (1434556-64-5)

Guidance literature:

With sodium hydrogencarbonate; In acetone; at 0 - 25 ℃; Inert atmosphere;

DOI:10.1021/jm400393u

Reference yield:

1-methyl-piperazine (109-01-3) → O2-(2,4-dinitro-5-fluorophenyl) 1-(4-methylpiperazin-1-yl)diazen-1-ium-1,2-diolate (1434556-64-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium methylate; titanium(IV) oxide; nitrogen(II) oxide / methanol; diethyl ether / 48 h / 25 °C / 760.05 Torr

2: sodium hydrogencarbonate / acetone / 0 - 25 °C / Inert atmosphere

With titanium(IV) oxide; nitrogen(II) oxide; sodium methylate; sodium hydrogencarbonate; In methanol; diethyl ether; acetone;

DOI:10.1021/jm400393u

Reference yield: 70.0%

O2-(2,4-dinitro-5-fluorophenyl) 1-(4-methylpiperazin-1-yl)diazen-1-ium-1,2-diolate (1434556-64-5) + C39H63NO9 → C50H75N7O15 (1434558-16-3)

Guidance literature:

With sodium carbonate; In tetrahydrofuran; at 25 ℃;

DOI:10.1021/jm400393u

upstream raw materials:

1,5-difluoro-2,4-dinitrobenzene

1-methyl-piperazine

Downstream raw materials:

C₅₀H₇₅N₇O₁₅

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