1-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-alanyl-D-isoglutamine methyl ester

Base Information

Chemical Name:1-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-alanyl-D-isoglutamine methyl ester
CAS No.:76502-94-8
Molecular Formula:C₃₄H₄₄N₄O₁₁
Molecular Weight:684.744
Hs Code.:

Synonyms:1-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-alanyl-D-isoglutamine methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-alanyl-D-isoglutamine methyl ester

Chemical Property:

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Technology Process of 1-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-alanyl-D-isoglutamine methyl ester

There total 3 articles about 1-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-alanyl-D-isoglutamine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76491-69-5
benzyloxycarbonylalanyl-D-isoglutamine methyl ester

: 76502-94-8
1-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-alanyl-D-isoglutamine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: 1. ethyl chloroformate, N-ethylmorpholine / 1. 0 deg C, 5 min, DMF; 2. 0 deg C, 1 h; room temperature, 12 h

With N-ethylmorpholine;; chloroformic acid ethyl ester;

Reference yield:

: 13343-63-0
benzyl 4,6-O-benzylidene-2-acetylamino-2-deoxy-α-D-glucopyranoside

: 76502-94-8
1-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-alanyl-D-isoglutamine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1. Na-K alloy, NaI; 2. NaOH / 1. heating, 1 h, THF; 2. heating, 1 h, H₂O, methanol

2: 1. ethyl chloroformate, N-ethylmorpholine / 1. 0 deg C, 5 min, DMF; 2. 0 deg C, 1 h; room temperature, 12 h

With N-ethylmorpholine;; sodium hydroxide; potassium Sodium; chloroformic acid ethyl ester; sodium iodide;

Reference yield:

: 2862-03-5
Benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-<(R)-1-carboxyethyl>-α-D-glucopyranoside

: 76491-70-8
L-alanyl-D-isoglutamine-γ-methyl ester

: 76502-94-8
1-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-alanyl-D-isoglutamine methyl ester

Guidance literature:: With N-ethylmorpholine;; chloroformic acid ethyl ester; Yield given. Multistep reaction; 1. 0 deg C, 5 min, DMF; 2. 0 deg C, 1 h; room temperature, 12 h;